$23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation$

23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation

Membrane technology is dominating the industry as an attractive approach for biogas purification due to its outstanding performance. Recently, there have been intensive efforts in the development of better separation efficiency of membrane which include altering the materials and modifying the metho...

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Main Authors:	Alia Aqilah, Ghazali, Raj Krishna Roshan, Kanasan, Sunarti, Abd Rahman, Mohamad Syafiq, Abdul Wahab, Nadia Sofea, Hazleen, Norhidayana, Mandayar
Format:	Conference or Workshop Item
Language:	English
Published:	IOP Publishing 2019
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/27803/ http://umpir.ump.edu.my/id/eprint/27803/ http://umpir.ump.edu.my/id/eprint/27803/1/23%20fractional%20factorial%20design%20for%20polymer%20based%20thin%20film.pdf

id	ump-27803
recordtype	eprints
spelling	ump-278032020-02-11T08:18:57Z http://umpir.ump.edu.my/id/eprint/27803/ 23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation Alia Aqilah, Ghazali Raj Krishna Roshan, Kanasan Sunarti, Abd Rahman Mohamad Syafiq, Abdul Wahab Nadia Sofea, Hazleen Norhidayana, Mandayar TP Chemical technology Membrane technology is dominating the industry as an attractive approach for biogas purification due to its outstanding performance. Recently, there have been intensive efforts in the development of better separation efficiency of membrane which include altering the materials and modifying the methods in preparing the membrane. A well-formed membrane is when they achieved both high permeability and excellent separation ability. Therefore, this study is focusing on identifying the best processing factors in PVC/Pebax thin film composite (TFC) membrane development towards CO2/CH4 separation by employing 23 fractional factorial design (FFD). A total of three factors; immersion times (5 & 15 min), Pebax concentration (1 & 5 wt%) and number of coating layers (1 & 4) were chosen to run simultaneously with CO2 permeability and ideal selectivity as the responses for this study. The results show that the most influential factors that affect the permeability are immersion time and Pebax concentration, while for selectivity are Pebax concentration and number of coating layer. The best condition was known to maximize the permeability and selectivity. The identified conditions were immersion time for 15 min, Pebax concentration at 5wt% and 4 layers of coating which gave CO2 permeability and gas selectivity of 19612 Barrer and 7.15, respectively. The outcome of this study indicates that FFD was suitable to minimize and eliminate factors by considering the interaction among the factors involves in membrane film synthesis for excellent gas separation performance. Besides, the existence of Pebax layer was verified by visual interpretation using Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR). IOP Publishing 2019 Conference or Workshop Item PeerReviewed pdf en cc_by http://umpir.ump.edu.my/id/eprint/27803/1/23%20fractional%20factorial%20design%20for%20polymer%20based%20thin%20film.pdf Alia Aqilah, Ghazali and Raj Krishna Roshan, Kanasan and Sunarti, Abd Rahman and Mohamad Syafiq, Abdul Wahab and Nadia Sofea, Hazleen and Norhidayana, Mandayar (2019) 23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation. In: IOP Conference Series: Materials Science and Engineering, 1st ProSES Symposium 2019, 4 September 2019 , Kuantan, Pahang, Malaysia. pp. 1-16., 702 (012049). ISSN 1757-899X https://doi.org/10.1088/1757-899X/702/1/012049
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Alia Aqilah, Ghazali Raj Krishna Roshan, Kanasan Sunarti, Abd Rahman Mohamad Syafiq, Abdul Wahab Nadia Sofea, Hazleen Norhidayana, Mandayar 23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
description	Membrane technology is dominating the industry as an attractive approach for biogas purification due to its outstanding performance. Recently, there have been intensive efforts in the development of better separation efficiency of membrane which include altering the materials and modifying the methods in preparing the membrane. A well-formed membrane is when they achieved both high permeability and excellent separation ability. Therefore, this study is focusing on identifying the best processing factors in PVC/Pebax thin film composite (TFC) membrane development towards CO2/CH4 separation by employing 23 fractional factorial design (FFD). A total of three factors; immersion times (5 & 15 min), Pebax concentration (1 & 5 wt%) and number of coating layers (1 & 4) were chosen to run simultaneously with CO2 permeability and ideal selectivity as the responses for this study. The results show that the most influential factors that affect the permeability are immersion time and Pebax concentration, while for selectivity are Pebax concentration and number of coating layer. The best condition was known to maximize the permeability and selectivity. The identified conditions were immersion time for 15 min, Pebax concentration at 5wt% and 4 layers of coating which gave CO2 permeability and gas selectivity of 19612 Barrer and 7.15, respectively. The outcome of this study indicates that FFD was suitable to minimize and eliminate factors by considering the interaction among the factors involves in membrane film synthesis for excellent gas separation performance. Besides, the existence of Pebax layer was verified by visual interpretation using Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR).
format	Conference or Workshop Item
author	Alia Aqilah, Ghazali Raj Krishna Roshan, Kanasan Sunarti, Abd Rahman Mohamad Syafiq, Abdul Wahab Nadia Sofea, Hazleen Norhidayana, Mandayar
author_facet	Alia Aqilah, Ghazali Raj Krishna Roshan, Kanasan Sunarti, Abd Rahman Mohamad Syafiq, Abdul Wahab Nadia Sofea, Hazleen Norhidayana, Mandayar
author_sort	Alia Aqilah, Ghazali
title	23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
title_short	23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
title_full	23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
title_fullStr	23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
title_full_unstemmed	23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation
title_sort	23 fractional factorial design for polymer based thin film composite (tfc) membrane synthesis for co2/ch4 separation
publisher	IOP Publishing
publishDate	2019
url	http://umpir.ump.edu.my/id/eprint/27803/ http://umpir.ump.edu.my/id/eprint/27803/ http://umpir.ump.edu.my/id/eprint/27803/1/23%20fractional%20factorial%20design%20for%20polymer%20based%20thin%20film.pdf
first_indexed	2023-09-18T22:43:36Z
last_indexed	2023-09-18T22:43:36Z
_version_	1777417077779333120

23 fractional factorial design for polymer based thin film composite (TFC) membrane synthesis for CO2/CH4 separation

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