Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical p...
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Unique Research Publishers
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ump-244252019-03-20T01:25:20Z http://umpir.ump.edu.my/id/eprint/24425/ Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates Najihah, Jamil Hazlina, Husin Ahmad Waseem, Alfida Zachary, Aman Zulkafli, Hassan TP Chemical technology The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical partially crystalline materials, showing some phases of separation are characterized by a glass transition (Tg = 25-26 °C) related to the amorphous part of the material, followed by two endothermic peaks related to the melting point (Tm = 185-225) of the crystallites. Due to the same material (PVA) used, the main composition temperatures are close to each other (for peak I between 320 K and 350 K, and for peak II between 429 K and 430 K). Finally, FTIR confirmed that between the three materials P 100, P 87 and P 85, there were distinctness in the band absorbed between fully hydrolysed PVA, P 100 and partially hydrolysed PVA, P 85 and P 87. Unique Research Publishers 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24425/1/Characterization%20and%20preparation%20of%20Polyvinyl%20Alcohol%20%28PVA%29%20as%20inhibitor%20in%20formation%20of%20hydrates.pdf pdf en cc_by_4 http://umpir.ump.edu.my/id/eprint/24425/7/Characterization%20and%20preparation%20of%20Polyvinyl.pdf Najihah, Jamil and Hazlina, Husin and Ahmad Waseem, Alfida and Zachary, Aman and Zulkafli, Hassan (2018) Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates. International Journal of Current Science, Engineering & Technology, 1 (S1). pp. 578-584. ISSN 2581-4311 http://www.ijcrset.com/files/V1-S1-97.pdf |
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TP Chemical technology Najihah, Jamil Hazlina, Husin Ahmad Waseem, Alfida Zachary, Aman Zulkafli, Hassan Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
description |
The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical partially crystalline materials, showing some phases of separation are characterized by a glass transition (Tg = 25-26 °C) related to the amorphous part of the material, followed by two endothermic peaks related to the melting point (Tm = 185-225) of the crystallites. Due to the same material (PVA) used, the main composition temperatures are close to each other (for peak I between 320 K and 350 K, and for peak II between 429 K and 430 K). Finally, FTIR confirmed that between the three materials P 100, P 87 and P 85, there were distinctness in the band absorbed between fully hydrolysed PVA, P 100 and partially hydrolysed PVA, P 85 and P 87. |
format |
Article |
author |
Najihah, Jamil Hazlina, Husin Ahmad Waseem, Alfida Zachary, Aman Zulkafli, Hassan |
author_facet |
Najihah, Jamil Hazlina, Husin Ahmad Waseem, Alfida Zachary, Aman Zulkafli, Hassan |
author_sort |
Najihah, Jamil |
title |
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
title_short |
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
title_full |
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
title_fullStr |
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
title_full_unstemmed |
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates |
title_sort |
characterization and preparation of polyvinyl alcohol (pva) as inhibitor in formation of hydrates |
publisher |
Unique Research Publishers |
publishDate |
2018 |
url |
http://umpir.ump.edu.my/id/eprint/24425/ http://umpir.ump.edu.my/id/eprint/24425/ http://umpir.ump.edu.my/id/eprint/24425/1/Characterization%20and%20preparation%20of%20Polyvinyl%20Alcohol%20%28PVA%29%20as%20inhibitor%20in%20formation%20of%20hydrates.pdf http://umpir.ump.edu.my/id/eprint/24425/7/Characterization%20and%20preparation%20of%20Polyvinyl.pdf |
first_indexed |
2023-09-18T22:36:57Z |
last_indexed |
2023-09-18T22:36:57Z |
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1777416659503415296 |