Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates

The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical p...

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Main Authors: Najihah, Jamil, Hazlina, Husin, Ahmad Waseem, Alfida, Zachary, Aman, Zulkafli, Hassan
Format: Article
Language:English
English
Published: Unique Research Publishers 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/24425/
http://umpir.ump.edu.my/id/eprint/24425/
http://umpir.ump.edu.my/id/eprint/24425/1/Characterization%20and%20preparation%20of%20Polyvinyl%20Alcohol%20%28PVA%29%20as%20inhibitor%20in%20formation%20of%20hydrates.pdf
http://umpir.ump.edu.my/id/eprint/24425/7/Characterization%20and%20preparation%20of%20Polyvinyl.pdf
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spelling ump-244252019-03-20T01:25:20Z http://umpir.ump.edu.my/id/eprint/24425/ Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates Najihah, Jamil Hazlina, Husin Ahmad Waseem, Alfida Zachary, Aman Zulkafli, Hassan TP Chemical technology The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical partially crystalline materials, showing some phases of separation are characterized by a glass transition (Tg = 25-26 °C) related to the amorphous part of the material, followed by two endothermic peaks related to the melting point (Tm = 185-225) of the crystallites. Due to the same material (PVA) used, the main composition temperatures are close to each other (for peak I between 320 K and 350 K, and for peak II between 429 K and 430 K). Finally, FTIR confirmed that between the three materials P 100, P 87 and P 85, there were distinctness in the band absorbed between fully hydrolysed PVA, P 100 and partially hydrolysed PVA, P 85 and P 87. Unique Research Publishers 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24425/1/Characterization%20and%20preparation%20of%20Polyvinyl%20Alcohol%20%28PVA%29%20as%20inhibitor%20in%20formation%20of%20hydrates.pdf pdf en cc_by_4 http://umpir.ump.edu.my/id/eprint/24425/7/Characterization%20and%20preparation%20of%20Polyvinyl.pdf Najihah, Jamil and Hazlina, Husin and Ahmad Waseem, Alfida and Zachary, Aman and Zulkafli, Hassan (2018) Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates. International Journal of Current Science, Engineering & Technology, 1 (S1). pp. 578-584. ISSN 2581-4311 http://www.ijcrset.com/files/V1-S1-97.pdf
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
Najihah, Jamil
Hazlina, Husin
Ahmad Waseem, Alfida
Zachary, Aman
Zulkafli, Hassan
Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
description The thermal properties of PVA with different degree of hydrolysis (DH) was studied by preparation of aqueous polymer solution, followed by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The DSC result showed the typical partially crystalline materials, showing some phases of separation are characterized by a glass transition (Tg = 25-26 °C) related to the amorphous part of the material, followed by two endothermic peaks related to the melting point (Tm = 185-225) of the crystallites. Due to the same material (PVA) used, the main composition temperatures are close to each other (for peak I between 320 K and 350 K, and for peak II between 429 K and 430 K). Finally, FTIR confirmed that between the three materials P 100, P 87 and P 85, there were distinctness in the band absorbed between fully hydrolysed PVA, P 100 and partially hydrolysed PVA, P 85 and P 87.
format Article
author Najihah, Jamil
Hazlina, Husin
Ahmad Waseem, Alfida
Zachary, Aman
Zulkafli, Hassan
author_facet Najihah, Jamil
Hazlina, Husin
Ahmad Waseem, Alfida
Zachary, Aman
Zulkafli, Hassan
author_sort Najihah, Jamil
title Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
title_short Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
title_full Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
title_fullStr Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
title_full_unstemmed Characterization and preparation of Polyvinyl Alcohol (PVA) as inhibitor in formation of hydrates
title_sort characterization and preparation of polyvinyl alcohol (pva) as inhibitor in formation of hydrates
publisher Unique Research Publishers
publishDate 2018
url http://umpir.ump.edu.my/id/eprint/24425/
http://umpir.ump.edu.my/id/eprint/24425/
http://umpir.ump.edu.my/id/eprint/24425/1/Characterization%20and%20preparation%20of%20Polyvinyl%20Alcohol%20%28PVA%29%20as%20inhibitor%20in%20formation%20of%20hydrates.pdf
http://umpir.ump.edu.my/id/eprint/24425/7/Characterization%20and%20preparation%20of%20Polyvinyl.pdf
first_indexed 2023-09-18T22:36:57Z
last_indexed 2023-09-18T22:36:57Z
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