Improved Fischer esterification of substituted benzoic acid under sealed-vessel microwave condition
Ethyl-4-fluoro-3-nitro benzoate was synthesised in good yield under closed vessel conditions using a single-mode microwave. This simple method involved adding catalytic amounts of H2SO4 at specific intervals of time to overcome the problems associated with equilibrium. The method was first optimised...
Main Authors: | Abd Hamid, Shafida, Hamzah, Nurasyikin, Abdul Rahim, Aisyah Saad |
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Format: | Article |
Language: | English |
Published: |
Penerbit Universiti Sains Malaysia
2015
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Subjects: | |
Online Access: | http://irep.iium.edu.my/46576/ http://irep.iium.edu.my/46576/1/Journal_of_Physical_Science%2C_Vol._26%282%29%2C_53%E2%80%9361%2C_2015.pdf |
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