Improved Fischer esterification of substituted benzoic acid under sealed-vessel microwave condition
Ethyl-4-fluoro-3-nitro benzoate was synthesised in good yield under closed vessel conditions using a single-mode microwave. This simple method involved adding catalytic amounts of H2SO4 at specific intervals of time to overcome the problems associated with equilibrium. The method was first optimised...
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Penerbit Universiti Sains Malaysia
2015
|
Subjects: | |
Online Access: | http://irep.iium.edu.my/46576/ http://irep.iium.edu.my/46576/1/Journal_of_Physical_Science%2C_Vol._26%282%29%2C_53%E2%80%9361%2C_2015.pdf |