Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol

Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distributi...

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Main Authors: Koay, Gregory F. L., Chuaha, Teong-Guan, Sumaiya, Zainal Abidin, Salmiah, Ahmad, Choonga, Thomas S. Y.
Format: Article
Language:English
English
Published: Elsevier 2012
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/6790/
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http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf
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spelling ump-67902018-04-18T01:14:08Z http://umpir.ump.edu.my/id/eprint/6790/ Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol Koay, Gregory F. L. Chuaha, Teong-Guan Sumaiya, Zainal Abidin Salmiah, Ahmad Choonga, Thomas S. Y. QD Chemistry Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distribution and purity were studied. The purity was higher, while the yield and particle size were lower and smaller, respectively, at higher temperature and solvent concentration. The solvent crystallization process efficiency was rated at 66–69% when carried out with 70–80% isopropyl alcohol at 20 ◦C. Elsevier 2012 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/6790/4/Particuology%2010.pdf Koay, Gregory F. L. and Chuaha, Teong-Guan and Sumaiya, Zainal Abidin and Salmiah, Ahmad and Choonga, Thomas S. Y. (2012) Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol. Particuology, 10 (1). pp. 127-131. http://www.sciencedirect.com/science/article/pii/S1674200111001714# 10.1016/j.partic.2011.04.011
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic QD Chemistry
spellingShingle QD Chemistry
Koay, Gregory F. L.
Chuaha, Teong-Guan
Sumaiya, Zainal Abidin
Salmiah, Ahmad
Choonga, Thomas S. Y.
Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
description Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distribution and purity were studied. The purity was higher, while the yield and particle size were lower and smaller, respectively, at higher temperature and solvent concentration. The solvent crystallization process efficiency was rated at 66–69% when carried out with 70–80% isopropyl alcohol at 20 ◦C.
format Article
author Koay, Gregory F. L.
Chuaha, Teong-Guan
Sumaiya, Zainal Abidin
Salmiah, Ahmad
Choonga, Thomas S. Y.
author_facet Koay, Gregory F. L.
Chuaha, Teong-Guan
Sumaiya, Zainal Abidin
Salmiah, Ahmad
Choonga, Thomas S. Y.
author_sort Koay, Gregory F. L.
title Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
title_short Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
title_full Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
title_fullStr Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
title_full_unstemmed Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
title_sort effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
publisher Elsevier
publishDate 2012
url http://umpir.ump.edu.my/id/eprint/6790/
http://umpir.ump.edu.my/id/eprint/6790/
http://umpir.ump.edu.my/id/eprint/6790/
http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf
http://umpir.ump.edu.my/id/eprint/6790/4/Particuology%2010.pdf
first_indexed 2023-09-18T22:02:52Z
last_indexed 2023-09-18T22:02:52Z
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