Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication

A key issue in the synthesis of molecular imprinted polymer nanoparticles is the identification and optimization of the main factors affecting the material structure and size. This paper describe an experimental design approach to synthesis bisphenol A molecular imprinted polymer nanoparticles (BPA-...

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Main Authors:	C. K. M., Faizal, Shareena, Mohd Sharif
Format:	Conference or Workshop Item
Language:	English
Published:	2011
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/5830/ http://umpir.ump.edu.my/id/eprint/5830/1/fkksa-2011-KuFaizal-Application_of_factorial_designSOMChe.pdf

id	ump-5830
recordtype	eprints
spelling	ump-58302018-01-12T02:59:02Z http://umpir.ump.edu.my/id/eprint/5830/ Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication C. K. M., Faizal Shareena, Mohd Sharif TP Chemical technology A key issue in the synthesis of molecular imprinted polymer nanoparticles is the identification and optimization of the main factors affecting the material structure and size. This paper describe an experimental design approach to synthesis bisphenol A molecular imprinted polymer nanoparticles (BPA-MIP NPs) aimed at analysis of the relationship of four selected parameters: the polymerisation temperature, agitation rate, cross-linker to solvent ratio, and percentage of initiator. The results presented demonstrate the importance of keeping the right balance between these various parameters of polymerisation conditions which are approximately 60oC, 100rpm, 65% solvent ratio and 1% initiator, respectively. Generally, it can be concluded that MIPs should be synthesized using enough heating, adequate agitation, low concentration of initiator and with a bit higher amount of solvent. Such procedure is proven as time and cost effective, and also can be used as a general tool in the preparation of MIP NPs for different target molecules. 2011 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/5830/1/fkksa-2011-KuFaizal-Application_of_factorial_designSOMChe.pdf C. K. M., Faizal and Shareena, Mohd Sharif (2011) Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication. In: Proceeding of International Conference Of Chemical Engineering And Industrial Biotechnology In Conjunction With 25th Symposium Of Malaysian Chemical Engineer (ICCEIB-Somche) 2011, 28 November - 1 December 2011 , Kuantan, Pahang. pp. 1-6..
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology C. K. M., Faizal Shareena, Mohd Sharif Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
description	A key issue in the synthesis of molecular imprinted polymer nanoparticles is the identification and optimization of the main factors affecting the material structure and size. This paper describe an experimental design approach to synthesis bisphenol A molecular imprinted polymer nanoparticles (BPA-MIP NPs) aimed at analysis of the relationship of four selected parameters: the polymerisation temperature, agitation rate, cross-linker to solvent ratio, and percentage of initiator. The results presented demonstrate the importance of keeping the right balance between these various parameters of polymerisation conditions which are approximately 60oC, 100rpm, 65% solvent ratio and 1% initiator, respectively. Generally, it can be concluded that MIPs should be synthesized using enough heating, adequate agitation, low concentration of initiator and with a bit higher amount of solvent. Such procedure is proven as time and cost effective, and also can be used as a general tool in the preparation of MIP NPs for different target molecules.
format	Conference or Workshop Item
author	C. K. M., Faizal Shareena, Mohd Sharif
author_facet	C. K. M., Faizal Shareena, Mohd Sharif
author_sort	C. K. M., Faizal
title	Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
title_short	Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
title_full	Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
title_fullStr	Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
title_full_unstemmed	Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication
title_sort	application of factorial design analysis to control bisphenol a mip fabrication
publishDate	2011
url	http://umpir.ump.edu.my/id/eprint/5830/ http://umpir.ump.edu.my/id/eprint/5830/1/fkksa-2011-KuFaizal-Application_of_factorial_designSOMChe.pdf
first_indexed	2023-09-18T22:01:14Z
last_indexed	2023-09-18T22:01:14Z
_version_	1777414412584353792

Application of Factorial Design Analysis to Control Bisphenol A MIP fabrication

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