Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol

Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. Th...

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Main Authors:	Khan, Maksudur R., Ong, Huei Ruey, Ridzuan, Ramli, R. M., Yunus
Format:	Article
Published:	Trans Tech Publications Inc. 2014
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/5378/ http://umpir.ump.edu.my/id/eprint/5378/ http://umpir.ump.edu.my/id/eprint/5378/

id	ump-5378
recordtype	eprints
spelling	ump-53782018-01-12T03:00:15Z http://umpir.ump.edu.my/id/eprint/5378/ Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol Khan, Maksudur R. Ong, Huei Ruey Ridzuan, Ramli R. M., Yunus TP Chemical technology Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. The experiment result showed that, 7.062 mM of hydrazine solution and 0.0147 mM of Cu2+ solution were needed to synthesize narrow size monodisperseCuNPs.The presence of nanoparticle was found after an induction period of 4 h and further reaction time, complete Cu0 state nanoparticle was obtained as deep red wine colour was observed. Stability study of CuNPs showed that the nanoparticles were stable up to 4 days. The particle size of the nanoparticles have been analysed by transmission electron microscopy (TEM) and the average size of CuNPs was in the range 2 to 10 nm. Trans Tech Publications Inc. 2014 Article PeerReviewed Khan, Maksudur R. and Ong, Huei Ruey and Ridzuan, Ramli and R. M., Yunus (2014) Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol. Applied Mechanics and Materials, 481. pp. 21-26. ISSN 1662-7482 http://dx.doi.org/10.4028/www.scientific.net/AMM.481.21 doi:10.4028/www.scientific.net/AMM.481.21
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
topic	TP Chemical technology
spellingShingle	TP Chemical technology Khan, Maksudur R. Ong, Huei Ruey Ridzuan, Ramli R. M., Yunus Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
description	Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. The experiment result showed that, 7.062 mM of hydrazine solution and 0.0147 mM of Cu2+ solution were needed to synthesize narrow size monodisperseCuNPs.The presence of nanoparticle was found after an induction period of 4 h and further reaction time, complete Cu0 state nanoparticle was obtained as deep red wine colour was observed. Stability study of CuNPs showed that the nanoparticles were stable up to 4 days. The particle size of the nanoparticles have been analysed by transmission electron microscopy (TEM) and the average size of CuNPs was in the range 2 to 10 nm.
format	Article
author	Khan, Maksudur R. Ong, Huei Ruey Ridzuan, Ramli R. M., Yunus
author_facet	Khan, Maksudur R. Ong, Huei Ruey Ridzuan, Ramli R. M., Yunus
author_sort	Khan, Maksudur R.
title	Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_short	Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_full	Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_fullStr	Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_full_unstemmed	Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_sort	synthesis of copper nanoparticles at room temperature using hydrazine in glycerol
publisher	Trans Tech Publications Inc.
publishDate	2014
url	http://umpir.ump.edu.my/id/eprint/5378/ http://umpir.ump.edu.my/id/eprint/5378/ http://umpir.ump.edu.my/id/eprint/5378/
first_indexed	2023-09-18T22:00:42Z
last_indexed	2023-09-18T22:00:42Z
_version_	1777414378461593600

Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol

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