Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide
Eliminating soluble lead ion from wastewater through adsorption has been more critical with the nonstop anthropogenic activity releasing it as waste. This study focuses on synthesizing zinc oxide-modified graphene oxide (ZnO/GO) following the solvothermal method and evaluating its capacity in adsorb...
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ump-277482020-03-09T04:23:55Z http://umpir.ump.edu.my/id/eprint/27748/ Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide Siti Zu Nurain, Ahmad Wan Norharyati, Wan Salleh Norhaniza, Yusof Mohd Zamri, Mohd Yusopa Rafidah, Hamdan Nor Asikin, Awang Nor Hafiza, Ismail Norafiqah, Rosman Norazlianie, Sazali Ahmad Fauzi, Ismail Q Science (General) TP Chemical technology Eliminating soluble lead ion from wastewater through adsorption has been more critical with the nonstop anthropogenic activity releasing it as waste. This study focuses on synthesizing zinc oxide-modified graphene oxide (ZnO/GO) following the solvothermal method and evaluating its capacity in adsorbing Pb(II) ion. The synthesized ZnO/GO was characterized using X-ray Diffraction (XRD), Fourier-transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) analysis; the results revealed that the graphene oxide (GO) had successfully bonded with zinc oxide (ZnO). The adsorption of Pb(II) on the functionalized ZnO/GO was studied under different experimental conditions, which confirmed the high adsorption capacity of ZnO/GO in removing Pb(II). The optimum pH and adsorbent dosage of ZnO/GO were at pH 5 and 0.16 g/L and the maximum adsorption capacity reached 909.09 mg/g. The most rapid adsorption occurred in the first 30 minutes of contact time with the equilibrium time achieved in 160 minutes and the adsorption isotherm and kinetic followed the Langmuir and pseudo-first order model. Therefore, the newly synthesized ZnO/GO showed superior adsorption capacity for Pb(II) compared to its pure GO. Taylor & Francis 2020 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/27748/1/Ahmadetal.2020PbIIremovalZno_GO.pdf pdf en http://umpir.ump.edu.my/id/eprint/27748/7/Pb%28II%29%20removal%20and%20its%20adsorption%20from%20aqueous%20solution__abstract.pdf Siti Zu Nurain, Ahmad and Wan Norharyati, Wan Salleh and Norhaniza, Yusof and Mohd Zamri, Mohd Yusopa and Rafidah, Hamdan and Nor Asikin, Awang and Nor Hafiza, Ismail and Norafiqah, Rosman and Norazlianie, Sazali and Ahmad Fauzi, Ismail (2020) Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide. Chemical Engineering Communications. pp. 1-16. ISSN 1563-5201 (In Press) https://doi.org/10.1080/00986445.2020.1715957 https://doi.org/10.1080/00986445.2020.1715957 |
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Q Science (General) TP Chemical technology Siti Zu Nurain, Ahmad Wan Norharyati, Wan Salleh Norhaniza, Yusof Mohd Zamri, Mohd Yusopa Rafidah, Hamdan Nor Asikin, Awang Nor Hafiza, Ismail Norafiqah, Rosman Norazlianie, Sazali Ahmad Fauzi, Ismail Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
description |
Eliminating soluble lead ion from wastewater through adsorption has been more critical with the nonstop anthropogenic activity releasing it as waste. This study focuses on synthesizing zinc oxide-modified graphene oxide (ZnO/GO) following the solvothermal method and evaluating its capacity in adsorbing Pb(II) ion. The synthesized ZnO/GO was characterized using X-ray Diffraction (XRD), Fourier-transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) analysis; the results revealed that the graphene oxide (GO) had successfully bonded with zinc oxide (ZnO). The adsorption of Pb(II) on the functionalized ZnO/GO was studied under different experimental conditions, which confirmed the high adsorption capacity of ZnO/GO in removing Pb(II). The optimum pH and adsorbent dosage of ZnO/GO were at pH 5 and 0.16 g/L and the maximum adsorption capacity reached 909.09 mg/g. The most rapid adsorption occurred in the first 30 minutes of contact time with the equilibrium time achieved in 160 minutes and the adsorption isotherm and kinetic followed the Langmuir and pseudo-first order model. Therefore, the newly synthesized ZnO/GO showed superior adsorption capacity for Pb(II) compared to its pure GO. |
format |
Article |
author |
Siti Zu Nurain, Ahmad Wan Norharyati, Wan Salleh Norhaniza, Yusof Mohd Zamri, Mohd Yusopa Rafidah, Hamdan Nor Asikin, Awang Nor Hafiza, Ismail Norafiqah, Rosman Norazlianie, Sazali Ahmad Fauzi, Ismail |
author_facet |
Siti Zu Nurain, Ahmad Wan Norharyati, Wan Salleh Norhaniza, Yusof Mohd Zamri, Mohd Yusopa Rafidah, Hamdan Nor Asikin, Awang Nor Hafiza, Ismail Norafiqah, Rosman Norazlianie, Sazali Ahmad Fauzi, Ismail |
author_sort |
Siti Zu Nurain, Ahmad |
title |
Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
title_short |
Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
title_full |
Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
title_fullStr |
Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
title_full_unstemmed |
Pb(II) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
title_sort |
pb(ii) removal and its adsorption from aqueous solution using zinc oxide/graphene oxide |
publisher |
Taylor & Francis |
publishDate |
2020 |
url |
http://umpir.ump.edu.my/id/eprint/27748/ http://umpir.ump.edu.my/id/eprint/27748/ http://umpir.ump.edu.my/id/eprint/27748/ http://umpir.ump.edu.my/id/eprint/27748/1/Ahmadetal.2020PbIIremovalZno_GO.pdf http://umpir.ump.edu.my/id/eprint/27748/7/Pb%28II%29%20removal%20and%20its%20adsorption%20from%20aqueous%20solution__abstract.pdf |
first_indexed |
2023-09-18T22:43:33Z |
last_indexed |
2023-09-18T22:43:33Z |
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1777417074192154624 |