Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent

In this study, ZnO nanoparticles were produced via the precipitating method supplemented by the microwave heating method. Zinc nitrate, sodium hydroxide and gum arabic were used as zinc salt, reducing agent and stabilizing agent respectively. The objective of this work is to investigate the pH effe...

Full description

Bibliographic Details
Main Authors:	Norlin, Pauzi, Norashikin, Mat Zain, Nurul Amira, Ahmad Yusof
Format:	Article
Language:	English
Published:	Penerbit UMT 2019
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/25098/ http://umpir.ump.edu.my/id/eprint/25098/ http://umpir.ump.edu.my/id/eprint/25098/1/Role%20of%20pH%20on%20zinc%20oxide%20nanoparticles.pdf

id	ump-25098
recordtype	eprints
spelling	ump-250982019-06-14T01:34:47Z http://umpir.ump.edu.my/id/eprint/25098/ Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent Norlin, Pauzi Norashikin, Mat Zain Nurul Amira, Ahmad Yusof TP Chemical technology In this study, ZnO nanoparticles were produced via the precipitating method supplemented by the microwave heating method. Zinc nitrate, sodium hydroxide and gum arabic were used as zinc salt, reducing agent and stabilizing agent respectively. The objective of this work is to investigate the pH effect, ranging from 5 to 12 on the ZnO nanoparticle size. By using Dynamic Light Scattering (DLS) method, the average nanoparticle size ranged from 200 nm to 350 nm was obtained. UV-vis absorption spectrum was found in the range of 340 nm – 350 nm indicating the absorption peak of ZnO nanoparticles. FTIR spectra showed peaks range from 412 to 466 cm-1 which indicating standard of Zn–O stretching. The presence of (100), (002) and (101) planes were apparent in the XRD result, indicating the crystalline phase of ZnO nanoparticles. At the pH < 7, zinc nitrate hydroxide hydrate was produced, which was similar to ZnO nanoparticle that is in white solution. pH 10 was required to attain the pure phase of ZnO nanoparticles. Smaller nanoparticles synthesized at pH 10 show larger antibacterial effects at both Gram-positive bacterium, Staphylococcus aureus and Gram-negative bacterium, Escherichia coli. Penerbit UMT 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/25098/1/Role%20of%20pH%20on%20zinc%20oxide%20nanoparticles.pdf Norlin, Pauzi and Norashikin, Mat Zain and Nurul Amira, Ahmad Yusof (2019) Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent. Journal of Sustainability Science and Management, 14 (2). pp. 11-20. ISSN 2672-7226 http://jssm.umt.edu.my/wp-content/uploads/sites/51/2019/05/TABLE-OF-CONTENTS-JSSM-14.2.pdf
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Norlin, Pauzi Norashikin, Mat Zain Nurul Amira, Ahmad Yusof Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
description	In this study, ZnO nanoparticles were produced via the precipitating method supplemented by the microwave heating method. Zinc nitrate, sodium hydroxide and gum arabic were used as zinc salt, reducing agent and stabilizing agent respectively. The objective of this work is to investigate the pH effect, ranging from 5 to 12 on the ZnO nanoparticle size. By using Dynamic Light Scattering (DLS) method, the average nanoparticle size ranged from 200 nm to 350 nm was obtained. UV-vis absorption spectrum was found in the range of 340 nm – 350 nm indicating the absorption peak of ZnO nanoparticles. FTIR spectra showed peaks range from 412 to 466 cm-1 which indicating standard of Zn–O stretching. The presence of (100), (002) and (101) planes were apparent in the XRD result, indicating the crystalline phase of ZnO nanoparticles. At the pH < 7, zinc nitrate hydroxide hydrate was produced, which was similar to ZnO nanoparticle that is in white solution. pH 10 was required to attain the pure phase of ZnO nanoparticles. Smaller nanoparticles synthesized at pH 10 show larger antibacterial effects at both Gram-positive bacterium, Staphylococcus aureus and Gram-negative bacterium, Escherichia coli.
format	Article
author	Norlin, Pauzi Norashikin, Mat Zain Nurul Amira, Ahmad Yusof
author_facet	Norlin, Pauzi Norashikin, Mat Zain Nurul Amira, Ahmad Yusof
author_sort	Norlin, Pauzi
title	Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
title_short	Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
title_full	Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
title_fullStr	Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
title_full_unstemmed	Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
title_sort	role of ph on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent
publisher	Penerbit UMT
publishDate	2019
url	http://umpir.ump.edu.my/id/eprint/25098/ http://umpir.ump.edu.my/id/eprint/25098/ http://umpir.ump.edu.my/id/eprint/25098/1/Role%20of%20pH%20on%20zinc%20oxide%20nanoparticles.pdf
first_indexed	2023-09-18T22:38:22Z
last_indexed	2023-09-18T22:38:22Z
_version_	1777416748013715456

Role of pH on zinc oxide nanoparticles synthesis using gum arabic for sustainable and safe antibacterial agent

Similar Items