Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation

The traditional ways in the extraction of bioactive compounds using conventional methods are disadvantageous from both economic and environmental perspectives. In this, the potential of microwave-assisted hydrodistillation conditions for extraction of phytosterol from legume pods was investigated. S...

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Main Authors:	Noormazlinah, Ahmad, Norlaili, Hashim, Nour, A. H., Mimi Sakinah, A. M., Almajano, María Pilar, Nurul, Bahirah
Format:	Article
Language:	English
Published:	Department of Chemistry, Universitas Gadjah Mada Yogyakarta 2019
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/1/Extraction%20of%20Phytosterol%20Concentration%20in%20Different%20Legume.pdf

id	ump-25070
recordtype	eprints
spelling	ump-250702019-06-13T02:45:16Z http://umpir.ump.edu.my/id/eprint/25070/ Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation Noormazlinah, Ahmad Norlaili, Hashim Nour, A. H. Mimi Sakinah, A. M. Almajano, María Pilar Nurul, Bahirah TP Chemical technology The traditional ways in the extraction of bioactive compounds using conventional methods are disadvantageous from both economic and environmental perspectives. In this, the potential of microwave-assisted hydrodistillation conditions for extraction of phytosterol from legume pods was investigated. Salkowski test performed on the legume pod has shown the reddish brown in all sample which confirmed the presence of phytosterol qualitatively. Liebermann-Burchard procedure and ultraviolet-visible spectroscopy (UV-Vis) apparatus were used to study the concentration of phytosterol at different extraction parameters which are temperature (25–80 °C), solvent concentration (50–100% v/v), irradiation time (1–10 min) and microwave power (400–800 W). The optimal conditions for highest yield of extract (0.219 mg/L) were obtained at a microwave power of 600 W, the irradiation time of 6 min, and ethanol concentration of 75% v/v. Results obtained in this study have shown the capability of microwave-assisted hydrodistillation in the extraction of phytosterol from legume pod. Further works are nevertheless required to provide a deeper understanding of the mechanisms involved to facilitate the development of an optimum system applicable to the industry. Department of Chemistry, Universitas Gadjah Mada Yogyakarta 2019 Article PeerReviewed pdf en cc_by_nc_nd_4 http://umpir.ump.edu.my/id/eprint/25070/1/Extraction%20of%20Phytosterol%20Concentration%20in%20Different%20Legume.pdf Noormazlinah, Ahmad and Norlaili, Hashim and Nour, A. H. and Mimi Sakinah, A. M. and Almajano, María Pilar and Nurul, Bahirah (2019) Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation. Indonesian Journal of Chemistry, 19 (3). pp. 796-803. ISSN 1411-9420 (Print); 2460-1578 (Online) https://doi.org/10.22146/ijc.40865 https://doi.org/10.22146/ijc.40865
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Noormazlinah, Ahmad Norlaili, Hashim Nour, A. H. Mimi Sakinah, A. M. Almajano, María Pilar Nurul, Bahirah Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
description	The traditional ways in the extraction of bioactive compounds using conventional methods are disadvantageous from both economic and environmental perspectives. In this, the potential of microwave-assisted hydrodistillation conditions for extraction of phytosterol from legume pods was investigated. Salkowski test performed on the legume pod has shown the reddish brown in all sample which confirmed the presence of phytosterol qualitatively. Liebermann-Burchard procedure and ultraviolet-visible spectroscopy (UV-Vis) apparatus were used to study the concentration of phytosterol at different extraction parameters which are temperature (25–80 °C), solvent concentration (50–100% v/v), irradiation time (1–10 min) and microwave power (400–800 W). The optimal conditions for highest yield of extract (0.219 mg/L) were obtained at a microwave power of 600 W, the irradiation time of 6 min, and ethanol concentration of 75% v/v. Results obtained in this study have shown the capability of microwave-assisted hydrodistillation in the extraction of phytosterol from legume pod. Further works are nevertheless required to provide a deeper understanding of the mechanisms involved to facilitate the development of an optimum system applicable to the industry.
format	Article
author	Noormazlinah, Ahmad Norlaili, Hashim Nour, A. H. Mimi Sakinah, A. M. Almajano, María Pilar Nurul, Bahirah
author_facet	Noormazlinah, Ahmad Norlaili, Hashim Nour, A. H. Mimi Sakinah, A. M. Almajano, María Pilar Nurul, Bahirah
author_sort	Noormazlinah, Ahmad
title	Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
title_short	Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
title_full	Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
title_fullStr	Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
title_full_unstemmed	Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation
title_sort	extraction of phytosterol concentration in different legume pods by using microwave-assisted hydrodistillation
publisher	Department of Chemistry, Universitas Gadjah Mada Yogyakarta
publishDate	2019
url	http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/ http://umpir.ump.edu.my/id/eprint/25070/1/Extraction%20of%20Phytosterol%20Concentration%20in%20Different%20Legume.pdf
first_indexed	2023-09-18T22:38:18Z
last_indexed	2023-09-18T22:38:18Z
_version_	1777416744303853568

Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation

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