Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell

Cockle shell wastes are abundant, easily available and can be obtained at low cost. It is rich in calcium carbonate (CaCO3) that can be precursor to synthesis hydroxyapatite (HAP). The HAP has potential to be used in numerous applications such as biomedical and wastewater treatment. The overall obje...

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Main Authors:	Siti Hajar, Saharudin, Jun Haslinda, Haji Shariffuddin, Noor Ida Amalina, Ahamad Nordin, Aqeela, Ismail
Format:	Article
Language:	English
Published:	Elsevier Ltd 2019
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/1/Effect%20of%20aging%20time.pdf

id	ump-24984
recordtype	eprints
spelling	ump-249842020-01-29T04:22:08Z http://umpir.ump.edu.my/id/eprint/24984/ Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell Siti Hajar, Saharudin Jun Haslinda, Haji Shariffuddin Noor Ida Amalina, Ahamad Nordin Aqeela, Ismail TP Chemical technology Cockle shell wastes are abundant, easily available and can be obtained at low cost. It is rich in calcium carbonate (CaCO3) that can be precursor to synthesis hydroxyapatite (HAP). The HAP has potential to be used in numerous applications such as biomedical and wastewater treatment. The overall objective of this study is to determine the effect of aging time on the production of HAP derived from cockle shells waste. There are two aging times used in this study which are 3 and 5 h. The processes involved in synthesizing HAP were pretreatment of the cockle shells, production of CaCO3 in aragonite form, calcination of the CaCO3 to form CaO, production of Ca(OH)2 and finally reaction of the Ca(OH)2 solution with the phosphate source to obtain HAP. All samples have undergone physicochemical analyses to determine their phases, crystallinity, purity, functional group, surface morphology and elemental analysis using X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscope (SEM) and Electron Dispersive X-ray Analysis (EDX). This study found that 5 h aging time produced higher crystalline HAP compared to the others. Overall, this study proved that aging time play vital role in the quality of the synthesized HAP. Elsevier Ltd 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24984/1/Effect%20of%20aging%20time.pdf Siti Hajar, Saharudin and Jun Haslinda, Haji Shariffuddin and Noor Ida Amalina, Ahamad Nordin and Aqeela, Ismail (2019) Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell. Materials Today: Proceedings, 19 (Part 4). pp. 1208-1215. ISSN 2214-7853 https://doi.org/10.1016/j.matpr.2019.11.124 https://doi.org/10.1016/j.matpr.2019.11.124
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Siti Hajar, Saharudin Jun Haslinda, Haji Shariffuddin Noor Ida Amalina, Ahamad Nordin Aqeela, Ismail Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
description	Cockle shell wastes are abundant, easily available and can be obtained at low cost. It is rich in calcium carbonate (CaCO3) that can be precursor to synthesis hydroxyapatite (HAP). The HAP has potential to be used in numerous applications such as biomedical and wastewater treatment. The overall objective of this study is to determine the effect of aging time on the production of HAP derived from cockle shells waste. There are two aging times used in this study which are 3 and 5 h. The processes involved in synthesizing HAP were pretreatment of the cockle shells, production of CaCO3 in aragonite form, calcination of the CaCO3 to form CaO, production of Ca(OH)2 and finally reaction of the Ca(OH)2 solution with the phosphate source to obtain HAP. All samples have undergone physicochemical analyses to determine their phases, crystallinity, purity, functional group, surface morphology and elemental analysis using X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscope (SEM) and Electron Dispersive X-ray Analysis (EDX). This study found that 5 h aging time produced higher crystalline HAP compared to the others. Overall, this study proved that aging time play vital role in the quality of the synthesized HAP.
format	Article
author	Siti Hajar, Saharudin Jun Haslinda, Haji Shariffuddin Noor Ida Amalina, Ahamad Nordin Aqeela, Ismail
author_facet	Siti Hajar, Saharudin Jun Haslinda, Haji Shariffuddin Noor Ida Amalina, Ahamad Nordin Aqeela, Ismail
author_sort	Siti Hajar, Saharudin
title	Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
title_short	Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
title_full	Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
title_fullStr	Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
title_full_unstemmed	Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell
title_sort	effect of aging time in the synthesis of biogenic hydroxyapatite derived from cockle shell
publisher	Elsevier Ltd
publishDate	2019
url	http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/ http://umpir.ump.edu.my/id/eprint/24984/1/Effect%20of%20aging%20time.pdf
first_indexed	2023-09-18T22:38:07Z
last_indexed	2023-09-18T22:38:07Z
_version_	1777416732695068672

Effect of Aging Time in the Synthesis of Biogenic Hydroxyapatite Derived from Cockle Shell

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