Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)

In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxi...

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Main Authors: Muhammad Arif Fahmi, Supian, Khairatun Najwa, Mohd Amin, Saidatul Shima, Jamari, Shahril, Mohamad
Format: Article
Language:English
Published: Universiti Malaysia Pahang 2018
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Online Access:http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf
id ump-24430
recordtype eprints
spelling ump-244302019-03-19T04:10:48Z http://umpir.ump.edu.my/id/eprint/24430/ Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB) Muhammad Arif Fahmi, Supian Khairatun Najwa, Mohd Amin Saidatul Shima, Jamari Shahril, Mohamad TP Chemical technology In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxide (NaOH) concentration in alkaline pretreatment. The obtained optimum consistency and alkaline concentration are 5% and 20% respectively. The physicochemical and morphological characteristics, elemental composition and size distribution of the obtained alpha cellulose and MCC were analyzed in this work. Fourier transform infrared spectroscopy (FTIR) analysis provided clear evidence that the characteristic peak of lignin and hemicellulose were absent in the spectrum of the alpha cellulose and MCC. The difference in surface morphology and aggregation between alpha cellulose, MCC and commercialized MCC were observed by scanning electron microscopy (SEM). The mean length of approximately 251.3 μm, 41.4 μm and 138.6 μm were measured for alpha cellulose, MCC and commercialized MCC respectively. Thus, the isolated MCC from EFB has a good potential to be utilized as reinforcing agent in green composites and may be a precursor for future roselle derived nanocellulose, and thus a promising subject in nanocomposite research. Universiti Malaysia Pahang 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf Muhammad Arif Fahmi, Supian and Khairatun Najwa, Mohd Amin and Saidatul Shima, Jamari and Shahril, Mohamad (2018) Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB). Journal of Chemical Engineering and Industrial Biotechnology (JCEIB), 3. pp. 87-96. ISSN 0126-8139 http://jceib.ump.edu.my/index.php/en/volume-3-docman/89-investigation-on-pre-treatment-process-in-microcrystalline-cellulose-mcc-from-oil-palm-empty-fruit-bunch-efb https://doi.org/10.15282/JCEIB-V3-09.28/3/2018/3.3
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
description In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxide (NaOH) concentration in alkaline pretreatment. The obtained optimum consistency and alkaline concentration are 5% and 20% respectively. The physicochemical and morphological characteristics, elemental composition and size distribution of the obtained alpha cellulose and MCC were analyzed in this work. Fourier transform infrared spectroscopy (FTIR) analysis provided clear evidence that the characteristic peak of lignin and hemicellulose were absent in the spectrum of the alpha cellulose and MCC. The difference in surface morphology and aggregation between alpha cellulose, MCC and commercialized MCC were observed by scanning electron microscopy (SEM). The mean length of approximately 251.3 μm, 41.4 μm and 138.6 μm were measured for alpha cellulose, MCC and commercialized MCC respectively. Thus, the isolated MCC from EFB has a good potential to be utilized as reinforcing agent in green composites and may be a precursor for future roselle derived nanocellulose, and thus a promising subject in nanocomposite research.
format Article
author Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
author_facet Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
author_sort Muhammad Arif Fahmi, Supian
title Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_short Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_full Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_fullStr Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_full_unstemmed Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_sort investigation on pre-treatment process in microcrystalline cellulose (mcc) from oil palm empty fruit bunch (efb)
publisher Universiti Malaysia Pahang
publishDate 2018
url http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf
first_indexed 2023-09-18T22:36:58Z
last_indexed 2023-09-18T22:36:58Z
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