Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation

Corn-cobs are an agro-industrial waste and composed of cellulose mostly. In this study cellulose was isolated from the waste corn-cobs and modified to polymeric hydroxamic acid palladium complex 1 and characterized by using a variety of spectroscopic methods such as field emission scanning electron...

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Main Authors:	Sarkar, Shaheen M., Rashid, S. S., Karim, Kaykobad Md Rezaul, Siti Noor Hidayah, Mustapha, Yuen, Mei Lian, Normaiza, Z., Normaiza, Z, Khan, Maksudur R., Rahman, Md. Lutfor
Format:	Article
Language:	English
Published:	American Scientific Publishers 2019
Subjects:	QD Chemistry
Online Access:	http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/1/Cellulose%20Supported%20Pd%28II%29%20Complex%20Catalyzed1.pdf

id	ump-24085
recordtype	eprints
spelling	ump-240852019-02-07T03:15:26Z http://umpir.ump.edu.my/id/eprint/24085/ Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation Sarkar, Shaheen M. Rashid, S. S. Karim, Kaykobad Md Rezaul Siti Noor Hidayah, Mustapha Yuen, Mei Lian Normaiza, Z. Normaiza, Z Khan, Maksudur R. Rahman, Md. Lutfor QD Chemistry Corn-cobs are an agro-industrial waste and composed of cellulose mostly. In this study cellulose was isolated from the waste corn-cobs and modified to polymeric hydroxamic acid palladium complex 1 and characterized by using a variety of spectroscopic methods such as field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and inductively coupled plasma atomic emission spectroscopy (ICP-AES). The complex 1 exhibited high catalytic activity towards Suzuki and Heck coupling reactions of activated and deactivated aryl halides to give the respective coupling products with high yield. Moreover, the complex 1 was recovered and recycled five times with no considerable loss of catalytic overall performance. American Scientific Publishers 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24085/1/Cellulose%20Supported%20Pd%28II%29%20Complex%20Catalyzed1.pdf Sarkar, Shaheen M. and Rashid, S. S. and Karim, Kaykobad Md Rezaul and Siti Noor Hidayah, Mustapha and Yuen, Mei Lian and Normaiza, Z. and Normaiza, Z and Khan, Maksudur R. and Rahman, Md. Lutfor (2019) Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation. Journal of Nanoscience and Nanotechnology, 19 (5). pp. 2856-2861. ISSN 1533-4880 (Print); 1533-4899 (Online) https://doi.org/10.1166/jnn.2019.16289 https://doi.org/10.1166/jnn.2019.16289
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	QD Chemistry
spellingShingle	QD Chemistry Sarkar, Shaheen M. Rashid, S. S. Karim, Kaykobad Md Rezaul Siti Noor Hidayah, Mustapha Yuen, Mei Lian Normaiza, Z. Normaiza, Z Khan, Maksudur R. Rahman, Md. Lutfor Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
description	Corn-cobs are an agro-industrial waste and composed of cellulose mostly. In this study cellulose was isolated from the waste corn-cobs and modified to polymeric hydroxamic acid palladium complex 1 and characterized by using a variety of spectroscopic methods such as field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and inductively coupled plasma atomic emission spectroscopy (ICP-AES). The complex 1 exhibited high catalytic activity towards Suzuki and Heck coupling reactions of activated and deactivated aryl halides to give the respective coupling products with high yield. Moreover, the complex 1 was recovered and recycled five times with no considerable loss of catalytic overall performance.
format	Article
author	Sarkar, Shaheen M. Rashid, S. S. Karim, Kaykobad Md Rezaul Siti Noor Hidayah, Mustapha Yuen, Mei Lian Normaiza, Z. Normaiza, Z Khan, Maksudur R. Rahman, Md. Lutfor
author_facet	Sarkar, Shaheen M. Rashid, S. S. Karim, Kaykobad Md Rezaul Siti Noor Hidayah, Mustapha Yuen, Mei Lian Normaiza, Z. Normaiza, Z Khan, Maksudur R. Rahman, Md. Lutfor
author_sort	Sarkar, Shaheen M.
title	Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
title_short	Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
title_full	Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
title_fullStr	Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
title_full_unstemmed	Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation
title_sort	cellulose supported pd(ii) complex catalyzed carbon-carbon bonds formation
publisher	American Scientific Publishers
publishDate	2019
url	http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/ http://umpir.ump.edu.my/id/eprint/24085/1/Cellulose%20Supported%20Pd%28II%29%20Complex%20Catalyzed1.pdf
first_indexed	2023-09-18T22:36:17Z
last_indexed	2023-09-18T22:36:17Z
_version_	1777416616987852800

Cellulose Supported Pd(II) Complex Catalyzed Carbon-Carbon Bonds Formation

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