Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates

separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for...

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Main Authors:	Norazlianie, Sazali, K., Kadirgama, W. N., W. Salleh, F. E., C. Othman, N. H., Ismail, A. F., Ismail
Format:	Conference or Workshop Item
Language:	English
Published:	2018
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/23866/ http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf

id	ump-23866
recordtype	eprints
spelling	ump-238662019-01-18T08:16:46Z http://umpir.ump.edu.my/id/eprint/23866/ Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates Norazlianie, Sazali K., Kadirgama W. N., W. Salleh F. E., C. Othman N. H., Ismail A. F., Ismail TP Chemical technology separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for a commercially available PI/NCC altered the final properties of the carbons produced. A large variety of TCMs for gas separation have been developed by simple carbonization of a PI/NCC deposited on a ceramic tubular support. In this study, heating rates (1, 3, 5, and 7 oC/min) and stabilization environment (Argon, Nitrogen, and Helium) were investigated and the effect on permeation were determined for all resultant TCMs. In recent study, the modifications on the carbonization parameters such as stabilization conditions and heating rates during fabrication of PI/NCC-based carbon membranes could affect their gas separation performance. It was observed that stabilization under Argon environment produced carbon membranes with high separation performance while heating rates of 3oC/min improved the membrane selectivity but reduced the membrane’s permeability. In literature, the rate of evolution of the volatile compounds can be determined by carbonization heating rate as it is believed could affect the microstructure of the carbon membranes [1]. The variation in carbonization heating rates have showed different gas separation results on the PI/NCC carbon membranes as represented in Table 1. The data obtained showed an average value from at least three different PI/NCC carbon membranes with small error analysis of ±10% for both selectivity and permeance value. 2018-08 Conference or Workshop Item PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf Norazlianie, Sazali and K., Kadirgama and W. N., W. Salleh and F. E., C. Othman and N. H., Ismail and A. F., Ismail (2018) Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates. In: 4th International Conference Of Chemical Engineering And Industrial Biotechnology (ICCEIB 2018), 1-2 Aug 2018 , Seri Pacific Hotel, Kuala Lumpur. pp. 261-262.. (Submitted)
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Norazlianie, Sazali K., Kadirgama W. N., W. Salleh F. E., C. Othman N. H., Ismail A. F., Ismail Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
description	separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for a commercially available PI/NCC altered the final properties of the carbons produced. A large variety of TCMs for gas separation have been developed by simple carbonization of a PI/NCC deposited on a ceramic tubular support. In this study, heating rates (1, 3, 5, and 7 oC/min) and stabilization environment (Argon, Nitrogen, and Helium) were investigated and the effect on permeation were determined for all resultant TCMs. In recent study, the modifications on the carbonization parameters such as stabilization conditions and heating rates during fabrication of PI/NCC-based carbon membranes could affect their gas separation performance. It was observed that stabilization under Argon environment produced carbon membranes with high separation performance while heating rates of 3oC/min improved the membrane selectivity but reduced the membrane’s permeability. In literature, the rate of evolution of the volatile compounds can be determined by carbonization heating rate as it is believed could affect the microstructure of the carbon membranes [1]. The variation in carbonization heating rates have showed different gas separation results on the PI/NCC carbon membranes as represented in Table 1. The data obtained showed an average value from at least three different PI/NCC carbon membranes with small error analysis of ±10% for both selectivity and permeance value.
format	Conference or Workshop Item
author	Norazlianie, Sazali K., Kadirgama W. N., W. Salleh F. E., C. Othman N. H., Ismail A. F., Ismail
author_facet	Norazlianie, Sazali K., Kadirgama W. N., W. Salleh F. E., C. Othman N. H., Ismail A. F., Ismail
author_sort	Norazlianie, Sazali
title	Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_short	Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_full	Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_fullStr	Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_full_unstemmed	Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_sort	hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
publishDate	2018
url	http://umpir.ump.edu.my/id/eprint/23866/ http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf
first_indexed	2023-09-18T22:35:56Z
last_indexed	2023-09-18T22:35:56Z
_version_	1777416595169083392

Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates

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