Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation

This paper studies the synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation method. The kenaf fibre was prepared using the hydrothermal carbonisation process. Inverse suspension polymerisation process involved two different solution mixtures; a...

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Main Authors: Munirah Ezzah, Tuan Zakaria, Saidatul Shima, Jamari, Suriati, Ghazali
Format: Article
Language:English
Published: Penerbit UMP 2017
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/1/2_Tuan%20Zakaria%20et%20al%282%29.pdf
id ump-21165
recordtype eprints
spelling ump-211652018-05-30T04:01:09Z http://umpir.ump.edu.my/id/eprint/21165/ Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation Munirah Ezzah, Tuan Zakaria Saidatul Shima, Jamari Suriati, Ghazali TP Chemical technology This paper studies the synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation method. The kenaf fibre was prepared using the hydrothermal carbonisation process. Inverse suspension polymerisation process involved two different solution mixtures; a continuous phase containing cyclohexane, span-80, and kenaf fibre filler and a dispersed phase containing partially neutralised acrylic acid, acrylamide, initiator APS, and crosslinker NN-Methylenebisacrylamide. Kenaf fibre filler addition was varied with different weight percentages (0.01- 0.05 wt%). Water absorption testing using the teabag method showed sample containing 0.04 wt% carbon filler had the highest and optimal percentage of water absorbency, 55.27 g/g while the sample containing 0.01 wt% carbon filler displayed the lowest percentage of water absorbency, 45.27 g/g. All SPC samples showed a higher rate of water absorbency compared to SAP sample which had 40.61 g/g of average water absorbency. The samples were characterised by FTIR, FESEM - EDX, Mastersizer. All synthesised samples produced were in spherical beads form. It can be concluded that kenaf fibre affects the enhancement of superabsorbent polymer performance. Penerbit UMP 2017-09 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/21165/1/2_Tuan%20Zakaria%20et%20al%282%29.pdf Munirah Ezzah, Tuan Zakaria and Saidatul Shima, Jamari and Suriati, Ghazali (2017) Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation. Journal of Mechanical Engineering and Sciences (JMES) , 11 (3). pp. 2794-2800. ISSN 2289-4659 (print); 2231-8380 (online) https://doi.org/10.15282/jmes.11.3.2017.2.0253 doi: 10.15282/jmes.11.3.2017.2.0253
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Suriati, Ghazali
Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
description This paper studies the synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation method. The kenaf fibre was prepared using the hydrothermal carbonisation process. Inverse suspension polymerisation process involved two different solution mixtures; a continuous phase containing cyclohexane, span-80, and kenaf fibre filler and a dispersed phase containing partially neutralised acrylic acid, acrylamide, initiator APS, and crosslinker NN-Methylenebisacrylamide. Kenaf fibre filler addition was varied with different weight percentages (0.01- 0.05 wt%). Water absorption testing using the teabag method showed sample containing 0.04 wt% carbon filler had the highest and optimal percentage of water absorbency, 55.27 g/g while the sample containing 0.01 wt% carbon filler displayed the lowest percentage of water absorbency, 45.27 g/g. All SPC samples showed a higher rate of water absorbency compared to SAP sample which had 40.61 g/g of average water absorbency. The samples were characterised by FTIR, FESEM - EDX, Mastersizer. All synthesised samples produced were in spherical beads form. It can be concluded that kenaf fibre affects the enhancement of superabsorbent polymer performance.
format Article
author Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Suriati, Ghazali
author_facet Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Suriati, Ghazali
author_sort Munirah Ezzah, Tuan Zakaria
title Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
title_short Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
title_full Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
title_fullStr Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
title_full_unstemmed Synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
title_sort synthesis of superabsorbent carbonaceous kenaf fibre filled polymer using inverse suspension polymerisation
publisher Penerbit UMP
publishDate 2017
url http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/
http://umpir.ump.edu.my/id/eprint/21165/1/2_Tuan%20Zakaria%20et%20al%282%29.pdf
first_indexed 2023-09-18T22:30:57Z
last_indexed 2023-09-18T22:30:57Z
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