Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena

The specification of the crystal product is usually given in terms of crystal size distribution (CSD). To this end, optimal cooling strategy is necessary to achieve the CSD. The direct design control involving analytical CSD estimator is one of the approaches that can be used to generate the set-poi...

Full description

Bibliographic Details
Main Authors:	Zakirah, Mohd Zahari, Siti Zubaidah, Adnan, K., Ramesh, Suriyati, Saleh, Noor Asma Fazli, Abdul Samad
Format:	Conference or Workshop Item
Language:	English
Published:	IOP Publishing 2018
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/1/Zahari_2018_IOP_Conf._Ser.%253A_Mater._Sci._Eng._318_012013.pdf

id	ump-21109
recordtype	eprints
spelling	ump-211092018-06-01T00:38:09Z http://umpir.ump.edu.my/id/eprint/21109/ Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena Zakirah, Mohd Zahari Siti Zubaidah, Adnan K., Ramesh Suriyati, Saleh Noor Asma Fazli, Abdul Samad TP Chemical technology The specification of the crystal product is usually given in terms of crystal size distribution (CSD). To this end, optimal cooling strategy is necessary to achieve the CSD. The direct design control involving analytical CSD estimator is one of the approaches that can be used to generate the set-point. However, the effects of temperature on the crystal growth rate are neglected in the estimator. Thus, the temperature dependence on the crystal growth rate needs to be considered in order to provide an accurate set-point. The objective of this work is to extend the analytical CSD estimator where Arrhenius expression is employed to cover the effects of temperature on the growth rate. The application of this work is demonstrated through a potassium sulphate crystallisation process. Based on specified target CSD, the extended estimator is capable of generating the required set-point where a proposed controller successfully maintained the operation at the set-point to achieve the target CSD. Comparison with other cooling strategies shows a reduction up to 18.2% of the total number of undesirable crystals generated from secondary nucleation using linear cooling strategy is achieved. IOP Publishing 2018 Conference or Workshop Item PeerReviewed application/pdf en cc_by http://umpir.ump.edu.my/id/eprint/21109/1/Zahari_2018_IOP_Conf._Ser.%253A_Mater._Sci._Eng._318_012013.pdf Zakirah, Mohd Zahari and Siti Zubaidah, Adnan and K., Ramesh and Suriyati, Saleh and Noor Asma Fazli, Abdul Samad (2018) Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena. In: IOP Conference Series: Materials Science and Engineering, Malaysian Technical Universities Conference on Engineering and Technology (MUCET 2017), 6-7 December 2017 , Penang, Malaysia. pp. 1-6., 318 (012013). ISSN 1757-899X https://doi.org/10.1088/1757-899X/318/1/012013 012013
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Zakirah, Mohd Zahari Siti Zubaidah, Adnan K., Ramesh Suriyati, Saleh Noor Asma Fazli, Abdul Samad Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
description	The specification of the crystal product is usually given in terms of crystal size distribution (CSD). To this end, optimal cooling strategy is necessary to achieve the CSD. The direct design control involving analytical CSD estimator is one of the approaches that can be used to generate the set-point. However, the effects of temperature on the crystal growth rate are neglected in the estimator. Thus, the temperature dependence on the crystal growth rate needs to be considered in order to provide an accurate set-point. The objective of this work is to extend the analytical CSD estimator where Arrhenius expression is employed to cover the effects of temperature on the growth rate. The application of this work is demonstrated through a potassium sulphate crystallisation process. Based on specified target CSD, the extended estimator is capable of generating the required set-point where a proposed controller successfully maintained the operation at the set-point to achieve the target CSD. Comparison with other cooling strategies shows a reduction up to 18.2% of the total number of undesirable crystals generated from secondary nucleation using linear cooling strategy is achieved.
format	Conference or Workshop Item
author	Zakirah, Mohd Zahari Siti Zubaidah, Adnan K., Ramesh Suriyati, Saleh Noor Asma Fazli, Abdul Samad
author_facet	Zakirah, Mohd Zahari Siti Zubaidah, Adnan K., Ramesh Suriyati, Saleh Noor Asma Fazli, Abdul Samad
author_sort	Zakirah, Mohd Zahari
title	Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
title_short	Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
title_full	Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
title_fullStr	Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
title_full_unstemmed	Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena
title_sort	supersaturation control using analytical crystal size distribution estimator for temperature dependent in nucleation and crystal growth phenomena
publisher	IOP Publishing
publishDate	2018
url	http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/ http://umpir.ump.edu.my/id/eprint/21109/1/Zahari_2018_IOP_Conf._Ser.%253A_Mater._Sci._Eng._318_012013.pdf
first_indexed	2023-09-18T22:30:51Z
last_indexed	2023-09-18T22:30:51Z
_version_	1777416275063996416

Supersaturation Control using Analytical Crystal Size Distribution Estimator for Temperature Dependent in Nucleation and Crystal Growth Phenomena

Similar Items