As-spun Bio-novolac Fibre Morphological Study based on Resin’s Physico-chemical Properties

Bio-novolac fibre made from phenol-formaldehyde derived oil palm empty fruit bunch (EFB) was produced using electrospinning method. The bio-novolac phenol-formaldehyde was prepared via liquefaction and resinification at two different molar ratios of formaldehyde to liquefied EFB (LEFB) (F:LEFB = 0.5...

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Bibliographic Details
Main Authors: Siti Noorul Aina, Ab Rahim, Sarani, Zakaria, Sharifah Nabihah, Syed Jaafar, Chin, Hua Chia, Rasidi, Roslan, Hatika, Kaco, Sinyee, Gan
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2017
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/19855/
http://umpir.ump.edu.my/id/eprint/19855/
http://umpir.ump.edu.my/id/eprint/19855/1/pdf_files/SM-PDF-46-9-2017/39%20Siti%20Noorul%20Aina.pdf
Description
Summary:Bio-novolac fibre made from phenol-formaldehyde derived oil palm empty fruit bunch (EFB) was produced using electrospinning method. The bio-novolac phenol-formaldehyde was prepared via liquefaction and resinification at two different molar ratios of formaldehyde to liquefied EFB (LEFB) (F:LEFB = 0.5:1 and 0.8:1). Electrospinning was applied to the bio-novolac phenol-formaldehyde (BPF) in order to form smooth and thin as-spun fibre. The BPF was electrospun at 15 kV and 15 cm distance between needle and collector at a flow rate of 0.5 mL/h. At lower molecular weight of BPF resin, beads formation was observed. The addition of poly(vinyl) butyral (Mw = 175,000 - 250,000) has improved the fibre formation with lesser beads hence produced more fibre. Polymer solution with higher molecular weight produced better quality fibre.