Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature

Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature

Sodium Bismuth Titanate is a prominent candidate for a lead-free piezoelectric material. In this research, Na0.5Bi0.5TiO3 was synthesized at different sintering temperature by sol-gel method in which the solutions were prepared by using sodium acetate CH3COONa, bismuth (III) acetate Bi(CH3COO)3, tet...

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Main Author: Nurazlin, Ahmad
Format: Undergraduates Project Papers
Language:English
English
English
English
Published: 2016
Subjects:
TA Engineering (General). Civil engineering (General)
Online Access:http://umpir.ump.edu.my/id/eprint/19277/
http://umpir.ump.edu.my/id/eprint/19277/
http://umpir.ump.edu.my/id/eprint/19277/1/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Table%20of%20contents.pdf
http://umpir.ump.edu.my/id/eprint/19277/3/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Abstract.pdf
http://umpir.ump.edu.my/id/eprint/19277/13/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Chapter%201.pdf
http://umpir.ump.edu.my/id/eprint/19277/16/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-References.pdf
id ump-19277
recordtype eprints
spelling ump-192772017-12-19T03:35:12Z http://umpir.ump.edu.my/id/eprint/19277/ Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature Nurazlin, Ahmad TA Engineering (General). Civil engineering (General) Sodium Bismuth Titanate is a prominent candidate for a lead-free piezoelectric material. In this research, Na0.5Bi0.5TiO3 was synthesized at different sintering temperature by sol-gel method in which the solutions were prepared by using sodium acetate CH3COONa, bismuth (III) acetate Bi(CH3COO)3, tetra-n-butyl titanate Ti(OC4H9)4, as starting materials. Acetic acid glacial and 2-methoxyethanol as solvents and acetylacetone as a reagent to stabilize tetra-n-butyl titanate. The obtained BNT powder was analyzed using XRD, FESEM, FTIR. The mechanical properties of BNT was determined by hardness testing to investigate the strength of the samples. Pellets have been formed and sintered at 940 oC, 960 oC, 980 oC, 1000 oC for 5 hours. The XRD analysis confirmed that the perovskite structure was obtained at each temperature.The effect of slightly different sintering temperature on the structural was studied in detail. FESEM analysis of pellets showed the well-developed grains having larger size at higher sintering temperature. Hardness analysis that was examined by using Rockwell hardness testing shows that hardness measurement increased as the sintering temperature increased due to the amount of strain or defect content in the compact powders. 2016-12 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/19277/1/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Table%20of%20contents.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19277/3/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Abstract.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19277/13/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Chapter%201.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19277/16/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-References.pdf Nurazlin, Ahmad (2016) Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature. Faculty of Industrial Sciences and Technology, Universiti Malaysia Pahang. http://iportal.ump.edu.my/lib/item?id=chamo:102331&theme=UMP2
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
English
English
topic TA Engineering (General). Civil engineering (General)
spellingShingle TA Engineering (General). Civil engineering (General)
Nurazlin, Ahmad
Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
description Sodium Bismuth Titanate is a prominent candidate for a lead-free piezoelectric material. In this research, Na0.5Bi0.5TiO3 was synthesized at different sintering temperature by sol-gel method in which the solutions were prepared by using sodium acetate CH3COONa, bismuth (III) acetate Bi(CH3COO)3, tetra-n-butyl titanate Ti(OC4H9)4, as starting materials. Acetic acid glacial and 2-methoxyethanol as solvents and acetylacetone as a reagent to stabilize tetra-n-butyl titanate. The obtained BNT powder was analyzed using XRD, FESEM, FTIR. The mechanical properties of BNT was determined by hardness testing to investigate the strength of the samples. Pellets have been formed and sintered at 940 oC, 960 oC, 980 oC, 1000 oC for 5 hours. The XRD analysis confirmed that the perovskite structure was obtained at each temperature.The effect of slightly different sintering temperature on the structural was studied in detail. FESEM analysis of pellets showed the well-developed grains having larger size at higher sintering temperature. Hardness analysis that was examined by using Rockwell hardness testing shows that hardness measurement increased as the sintering temperature increased due to the amount of strain or defect content in the compact powders.
format Undergraduates Project Papers
author Nurazlin, Ahmad
author_facet Nurazlin, Ahmad
author_sort Nurazlin, Ahmad
title Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
title_short Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
title_full Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
title_fullStr Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
title_full_unstemmed Synthesis and characterization of sodium bismuth titanate (Na0.5Bi0.5TiO3) ceramic by sol-gel method at different sintering temperature
title_sort synthesis and characterization of sodium bismuth titanate (na0.5bi0.5tio3) ceramic by sol-gel method at different sintering temperature
publishDate 2016
url http://umpir.ump.edu.my/id/eprint/19277/
http://umpir.ump.edu.my/id/eprint/19277/
http://umpir.ump.edu.my/id/eprint/19277/1/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Table%20of%20contents.pdf
http://umpir.ump.edu.my/id/eprint/19277/3/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Abstract.pdf
http://umpir.ump.edu.my/id/eprint/19277/13/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-Chapter%201.pdf
http://umpir.ump.edu.my/id/eprint/19277/16/Synthesis%20and%20characterization%20of%20sodium%20bismuth%20titanate%20%28Na0.5Bi0.5TiO3%29%20ceramic%20by%20sol-gel%20method%20at%20different%20sintering%20temperature%20-References.pdf
first_indexed 2023-09-18T22:27:38Z
last_indexed 2023-09-18T22:27:38Z
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