Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires

We have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Boric Aci...

Full description

Bibliographic Details
Main Authors:	Nurhanis Sofiah, Abd Ghafar, Ulakanathan, S., Wan Sharuzi, Wan Harun, Kananathan, J., Samykano, Mahendran, Nurul Akmal, Che Lah, Sudhakar, K., K., Kadirgama, W. K., Ngui, Siregar, J. P.
Format:	Conference or Workshop Item
Language:	English English
Published:	IOP Publishing Ltd 2017
Subjects:	QC Physics TJ Mechanical engineering and machinery TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/17895/ http://umpir.ump.edu.my/id/eprint/17895/ http://umpir.ump.edu.my/id/eprint/17895/1/fkm-2017-Kananathan-Influence%20of%20boric%20acid.pdf http://umpir.ump.edu.my/id/eprint/17895/7/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf

id	ump-17895
recordtype	eprints
spelling	ump-178952018-08-28T08:26:05Z http://umpir.ump.edu.my/id/eprint/17895/ Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires Nurhanis Sofiah, Abd Ghafar Ulakanathan, S. Wan Sharuzi, Wan Harun Kananathan, J. Samykano, Mahendran Nurul Akmal, Che Lah Sudhakar, K. K., Kadirgama W. K., Ngui Siregar, J. P. QC Physics TJ Mechanical engineering and machinery TP Chemical technology We have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Boric Acid (H3BO3) as a stabilizer. The mixture of both solutions creates electrolyte and utilized for the electrochemical deposition of Ni nanowires. During the experiment, the boric acid concentration varied between 5 g/L, 37.5 g/L and 60 g/L with a deposition temperature of 80 °C (constant). After the electrochemical deposition process, AAO templates were cleaned with distilled water before dissolution in Sodium Hydroxide (NaOH) solution to obtain the freestanding Ni nanowires. Physical properties of the synthesized Ni nanowires were analyzed using Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD). We elaborate the physical properties of obtained Ni nanowires by taking into account the effect of boric acid concentration on the surface morphology, growth length, elemental composition and crystal orientation crystal of the synthesized nickel nanowires. The finding exposes that the boric acid concentration does not influence all aspects in the physicals properties of the synthesized Ni nanowires. The boric acid concentration did not affect the surface texture and crystal orientation. However, shorter Ni nanowires obtained as the concentration of boric acid increased IOP Publishing Ltd 2017 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/17895/1/fkm-2017-Kananathan-Influence%20of%20boric%20acid.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/17895/7/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf Nurhanis Sofiah, Abd Ghafar and Ulakanathan, S. and Wan Sharuzi, Wan Harun and Kananathan, J. and Samykano, Mahendran and Nurul Akmal, Che Lah and Sudhakar, K. and K., Kadirgama and W. K., Ngui and Siregar, J. P. (2017) Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires. In: 4th International Conference on Mechanical Engineering Research, ICMER 2017, 1-2 August 2017 , Swiss Garden Hotel and SpaKuantan, Pahang; Malaysia. pp. 1-7., 257 (1). ISSN 17578981 https://doi.org/10.1088/1757-899X/257/1/012033
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English English
topic	QC Physics TJ Mechanical engineering and machinery TP Chemical technology
spellingShingle	QC Physics TJ Mechanical engineering and machinery TP Chemical technology Nurhanis Sofiah, Abd Ghafar Ulakanathan, S. Wan Sharuzi, Wan Harun Kananathan, J. Samykano, Mahendran Nurul Akmal, Che Lah Sudhakar, K. K., Kadirgama W. K., Ngui Siregar, J. P. Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
description	We have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Boric Acid (H3BO3) as a stabilizer. The mixture of both solutions creates electrolyte and utilized for the electrochemical deposition of Ni nanowires. During the experiment, the boric acid concentration varied between 5 g/L, 37.5 g/L and 60 g/L with a deposition temperature of 80 °C (constant). After the electrochemical deposition process, AAO templates were cleaned with distilled water before dissolution in Sodium Hydroxide (NaOH) solution to obtain the freestanding Ni nanowires. Physical properties of the synthesized Ni nanowires were analyzed using Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD). We elaborate the physical properties of obtained Ni nanowires by taking into account the effect of boric acid concentration on the surface morphology, growth length, elemental composition and crystal orientation crystal of the synthesized nickel nanowires. The finding exposes that the boric acid concentration does not influence all aspects in the physicals properties of the synthesized Ni nanowires. The boric acid concentration did not affect the surface texture and crystal orientation. However, shorter Ni nanowires obtained as the concentration of boric acid increased
format	Conference or Workshop Item
author	Nurhanis Sofiah, Abd Ghafar Ulakanathan, S. Wan Sharuzi, Wan Harun Kananathan, J. Samykano, Mahendran Nurul Akmal, Che Lah Sudhakar, K. K., Kadirgama W. K., Ngui Siregar, J. P.
author_facet	Nurhanis Sofiah, Abd Ghafar Ulakanathan, S. Wan Sharuzi, Wan Harun Kananathan, J. Samykano, Mahendran Nurul Akmal, Che Lah Sudhakar, K. K., Kadirgama W. K., Ngui Siregar, J. P.
author_sort	Nurhanis Sofiah, Abd Ghafar
title	Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
title_short	Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
title_full	Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
title_fullStr	Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
title_full_unstemmed	Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires
title_sort	influence of boric acid (h3bo3) concentration on the physical properties of electrochemical deposited nickel (ni) nanowires
publisher	IOP Publishing Ltd
publishDate	2017
url	http://umpir.ump.edu.my/id/eprint/17895/ http://umpir.ump.edu.my/id/eprint/17895/ http://umpir.ump.edu.my/id/eprint/17895/1/fkm-2017-Kananathan-Influence%20of%20boric%20acid.pdf http://umpir.ump.edu.my/id/eprint/17895/7/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf
first_indexed	2023-09-18T22:25:00Z
last_indexed	2023-09-18T22:25:00Z
_version_	1777415907180544000

Influence of boric acid (H3BO3) concentration on the physical properties of electrochemical deposited nickel (Ni) nanowires

Similar Items