Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers

Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers

Recently, common research on stimuli-responsive polymers comprising thermoresponsive polymers has been widely investigated. In this research study, the synthesis process parameters of poly(Nvinylcaprolactam) (PNVCL) a thermoresponsive polymer, has been engaged for optimization as an attempt. The res...

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Main Authors: Marwah Noori, Mohammed, Kamal, Yusoh, Jun Haslinda, Haji Shariffuddin
Format: Article
Language:English
Published: IOP Publishing Ltd 2016
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/1/Methodized%20Depiction%20of%20Design%20of%20Experiment%20for%20Parameters%20Optimization%20in%20Synthesis%20of%20Poly%28Nvinylcaprolactam%29%20Thermoresponsive%20Polymers.pdf
id ump-16760
recordtype eprints
spelling ump-167602018-05-23T05:34:02Z http://umpir.ump.edu.my/id/eprint/16760/ Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers Marwah Noori, Mohammed Kamal, Yusoh Jun Haslinda, Haji Shariffuddin TP Chemical technology Recently, common research on stimuli-responsive polymers comprising thermoresponsive polymers has been widely investigated. In this research study, the synthesis process parameters of poly(Nvinylcaprolactam) (PNVCL) a thermoresponsive polymer, has been engaged for optimization as an attempt. The response surface methodology (RSM), has been employed in the identification of the elevated factors affecting on PNVCL production conversion (%) yield. Four independent process variables including monomer concentration, initiator concentration, polymerization temperature and time were studied. Various polymerization combination factors consist of a set of experiment runs were discussed using the Box–Behnken approach in Minitab 16. The study efficiently established the procedure and recompenses of RSM, for the estimation of process response. The optimum value for the most significant (temperature and time) variables for maximum PNVCL conversion (%) yield were obtained to be ~80 °C and 92.5 min, respectively. Monomer and initiator concentrations were hardly effective on the (%) yield. IOP Publishing Ltd 2016 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/16760/1/Methodized%20Depiction%20of%20Design%20of%20Experiment%20for%20Parameters%20Optimization%20in%20Synthesis%20of%20Poly%28Nvinylcaprolactam%29%20Thermoresponsive%20Polymers.pdf Marwah Noori, Mohammed and Kamal, Yusoh and Jun Haslinda, Haji Shariffuddin (2016) Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers. Materials Research Express, 3 (12). ISSN 2053-1591 https://doi.org/10.1088/2053-1591/3/12/125302 DOI: 10.1088/2053-1591/3/12/125302
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Marwah Noori, Mohammed
Kamal, Yusoh
Jun Haslinda, Haji Shariffuddin
Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
description Recently, common research on stimuli-responsive polymers comprising thermoresponsive polymers has been widely investigated. In this research study, the synthesis process parameters of poly(Nvinylcaprolactam) (PNVCL) a thermoresponsive polymer, has been engaged for optimization as an attempt. The response surface methodology (RSM), has been employed in the identification of the elevated factors affecting on PNVCL production conversion (%) yield. Four independent process variables including monomer concentration, initiator concentration, polymerization temperature and time were studied. Various polymerization combination factors consist of a set of experiment runs were discussed using the Box–Behnken approach in Minitab 16. The study efficiently established the procedure and recompenses of RSM, for the estimation of process response. The optimum value for the most significant (temperature and time) variables for maximum PNVCL conversion (%) yield were obtained to be ~80 °C and 92.5 min, respectively. Monomer and initiator concentrations were hardly effective on the (%) yield.
format Article
author Marwah Noori, Mohammed
Kamal, Yusoh
Jun Haslinda, Haji Shariffuddin
author_facet Marwah Noori, Mohammed
Kamal, Yusoh
Jun Haslinda, Haji Shariffuddin
author_sort Marwah Noori, Mohammed
title Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
title_short Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
title_full Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
title_fullStr Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
title_full_unstemmed Methodized Depiction of Design of Experiment for Parameters Optimization in Synthesis of Poly(Nvinylcaprolactam) Thermoresponsive Polymers
title_sort methodized depiction of design of experiment for parameters optimization in synthesis of poly(nvinylcaprolactam) thermoresponsive polymers
publisher IOP Publishing Ltd
publishDate 2016
url http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/
http://umpir.ump.edu.my/id/eprint/16760/1/Methodized%20Depiction%20of%20Design%20of%20Experiment%20for%20Parameters%20Optimization%20in%20Synthesis%20of%20Poly%28Nvinylcaprolactam%29%20Thermoresponsive%20Polymers.pdf
first_indexed 2023-09-18T22:22:45Z
last_indexed 2023-09-18T22:22:45Z
_version_ 1777415766422847488

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