Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design

Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This pap...

Full description

Bibliographic Details
Main Authors: Mohamad Rizza, Othman, Umarul Imran, Amran, Gade Padu, Rangaiah
Format: Article
Language:English
English
Published: AIDIC Servizi 2015
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf
http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf
id ump-12837
recordtype eprints
spelling ump-128372018-03-09T07:16:03Z http://umpir.ump.edu.my/id/eprint/12837/ Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design Mohamad Rizza, Othman Umarul Imran, Amran Gade Padu, Rangaiah TP Chemical technology Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This paper presents an ED based optimization approach of a dividing wall column (DWC) model for industrial oleochemical fatty acid fractionation. Taguchi method of ED will be used for the optimization of the control variables for efficient fractionation of fatty acid cuts, namely light-cut (LC), middle-cut (MC) and heavy-cut (HC). The DWC model was developed in Aspen Plus software using a rigorous four-column configuration. It is used to identify sensitive parameters, simulate experimental layout trials and results validation. The process is designed to achieve product purity of >99 mol.% LC and MC, and >90 mol.% for HC. A step-by-step approach to process optimization using Taguchi method is presented along with the statistical analysis results and their interpretation. The ED output will help in understanding the interaction between variables and their effects. With its simple, fast and non-tedious approach, ED using Taguchi method could prove its significance in improving the performance of fatty acid fractionation using DWC for possible industrial application. AIDIC Servizi 2015 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf Mohamad Rizza, Othman and Umarul Imran, Amran and Gade Padu, Rangaiah (2015) Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design. Chemical Engineering Transactions, 45. pp. 925-930. ISSN 2283-9216 http://dx.doi.org/10.3303/CET1545155 DOI: 10.3303/CET1545155
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
description Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This paper presents an ED based optimization approach of a dividing wall column (DWC) model for industrial oleochemical fatty acid fractionation. Taguchi method of ED will be used for the optimization of the control variables for efficient fractionation of fatty acid cuts, namely light-cut (LC), middle-cut (MC) and heavy-cut (HC). The DWC model was developed in Aspen Plus software using a rigorous four-column configuration. It is used to identify sensitive parameters, simulate experimental layout trials and results validation. The process is designed to achieve product purity of >99 mol.% LC and MC, and >90 mol.% for HC. A step-by-step approach to process optimization using Taguchi method is presented along with the statistical analysis results and their interpretation. The ED output will help in understanding the interaction between variables and their effects. With its simple, fast and non-tedious approach, ED using Taguchi method could prove its significance in improving the performance of fatty acid fractionation using DWC for possible industrial application.
format Article
author Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
author_facet Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
author_sort Mohamad Rizza, Othman
title Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_short Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_full Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_fullStr Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_full_unstemmed Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_sort process optimization of dwc for fatty acid fractionation using taguchi methods of experimental design
publisher AIDIC Servizi
publishDate 2015
url http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/
http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf
http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf
first_indexed 2023-09-18T22:14:47Z
last_indexed 2023-09-18T22:14:47Z
_version_ 1777415265020018688