Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization

This study is about synthesis and characterization of gel-type polymer aqueous dispersion polymerization (ADP) that involved two types of dispersion polymerization methodology; one-stage aqueous dispersion polymerization and two-stage aqueous dispersion polymerization. The monomer and crosslinker we...

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Main Author:	Nur Atiqah , Mohamad
Format:	Undergraduates Project Papers
Language:	English English English
Published:	2015
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/11033/ http://umpir.ump.edu.my/id/eprint/11033/ http://umpir.ump.edu.my/id/eprint/11033/1/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29.pdf http://umpir.ump.edu.my/id/eprint/11033/2/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%201.pdf http://umpir.ump.edu.my/id/eprint/11033/3/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%203.pdf

id	ump-11033
recordtype	eprints
spelling	ump-110332015-11-03T00:01:43Z http://umpir.ump.edu.my/id/eprint/11033/ Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization Nur Atiqah , Mohamad TP Chemical technology This study is about synthesis and characterization of gel-type polymer aqueous dispersion polymerization (ADP) that involved two types of dispersion polymerization methodology; one-stage aqueous dispersion polymerization and two-stage aqueous dispersion polymerization. The monomer and crosslinker were used in this study are styrene and EGDMA. Mixture of styrene and solvent undergone under nitrogen atmosphere for one hour at 70 °C before EGDMA was added into the mixture. The reaction was continued further 23 hours before the final product obtained. The polymers are characterized by using FTIR and CHNOS analysis. For one-stage polymerization, the final product was successfully obtained after 24 hours of reaction. The result obtained was not in bead-like shape but in flakes-formed. For two-stage ADP, based on the result from FTIR for two-stage polymerization, it shows that there are functional group that has been identified; alkene and alcohol and phenols reflect to functional group in styrene and EGDMA. It is clearly shown that EGDMA and styrene are incorporated in the back bone of polymer. For elemental analysis, CHNOS shows that there are 6.97% of nitrogen, 88.56% of carbon, 7.66% of hydrogen and 0.01% of sulphur at temperature of 70 oC while at 72 oC is 93.73% of nitrogen, 82.07% of carbon, 6.67% of hydrogen and 0.23% of sulphur. In conclusion, the particles were obtained in broad particles size distribution and polydisperse by varying the temperature for the reaction in two-stage ADP. 2015 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/11033/1/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/11033/2/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%201.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/11033/3/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%203.pdf Nur Atiqah , Mohamad (2015) Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization. Faculty of Chemical & Natural Resources Engineering, Universiti Malaysia Pahang. http://iportal.ump.edu.my/lib/item?id=chamo:91268&theme=UMP2
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English English English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Nur Atiqah , Mohamad Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
description	This study is about synthesis and characterization of gel-type polymer aqueous dispersion polymerization (ADP) that involved two types of dispersion polymerization methodology; one-stage aqueous dispersion polymerization and two-stage aqueous dispersion polymerization. The monomer and crosslinker were used in this study are styrene and EGDMA. Mixture of styrene and solvent undergone under nitrogen atmosphere for one hour at 70 °C before EGDMA was added into the mixture. The reaction was continued further 23 hours before the final product obtained. The polymers are characterized by using FTIR and CHNOS analysis. For one-stage polymerization, the final product was successfully obtained after 24 hours of reaction. The result obtained was not in bead-like shape but in flakes-formed. For two-stage ADP, based on the result from FTIR for two-stage polymerization, it shows that there are functional group that has been identified; alkene and alcohol and phenols reflect to functional group in styrene and EGDMA. It is clearly shown that EGDMA and styrene are incorporated in the back bone of polymer. For elemental analysis, CHNOS shows that there are 6.97% of nitrogen, 88.56% of carbon, 7.66% of hydrogen and 0.01% of sulphur at temperature of 70 oC while at 72 oC is 93.73% of nitrogen, 82.07% of carbon, 6.67% of hydrogen and 0.23% of sulphur. In conclusion, the particles were obtained in broad particles size distribution and polydisperse by varying the temperature for the reaction in two-stage ADP.
format	Undergraduates Project Papers
author	Nur Atiqah , Mohamad
author_facet	Nur Atiqah , Mohamad
author_sort	Nur Atiqah , Mohamad
title	Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
title_short	Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
title_full	Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
title_fullStr	Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
title_full_unstemmed	Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
title_sort	synthesis and characterization of gel-type polymers via aqueous dispersion polymerization
publishDate	2015
url	http://umpir.ump.edu.my/id/eprint/11033/ http://umpir.ump.edu.my/id/eprint/11033/ http://umpir.ump.edu.my/id/eprint/11033/1/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29.pdf http://umpir.ump.edu.my/id/eprint/11033/2/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%201.pdf http://umpir.ump.edu.my/id/eprint/11033/3/FKKSA%20-%20NUR%20ATIQAH%20MOHAMAD%20%28CD8983%29%20CHAP%203.pdf
first_indexed	2023-09-18T22:11:20Z
last_indexed	2023-09-18T22:11:20Z
_version_	1777415047910260736

Synthesis and characterization of gel-type polymers via aqueous dispersion polymerization

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