Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature

Silver nanoparticles (AgNPs) is known as a particle of silver with size range is varied between 1 to 100 nm. Silver nanoparticles is widely use in biosensor and molecular labelling field. In the synthesis of AgNPs process, it is quite challenging to develop a controlled synthesis procedure in order...

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Main Authors: Suriati, Ghazali, Nurul F., Salim
Format: Conference or Workshop Item
Language:English
Published: 2015
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/10697/
http://umpir.ump.edu.my/id/eprint/10697/1/Green%20Synthesis%20of%20Silver%20Nanoparticle-%20Effect%20of%20Reaction%20pH%20and%20Temperature.pdf
id ump-10697
recordtype eprints
spelling ump-106972018-02-08T03:19:58Z http://umpir.ump.edu.my/id/eprint/10697/ Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature Suriati, Ghazali Nurul F., Salim TP Chemical technology Silver nanoparticles (AgNPs) is known as a particle of silver with size range is varied between 1 to 100 nm. Silver nanoparticles is widely use in biosensor and molecular labelling field. In the synthesis of AgNPs process, it is quite challenging to develop a controlled synthesis procedure in order to get the uniform nano size distribution. In this study, uniform and well-dispersed silver nanoparticles were prepared by a simple and green chemical reduction method. The particles were synthesized via the reduction of silver nitrate by the presence of glucose and ascorbic acid as reducing agent and surfactant, respectively. The reaction pH, temperature and time could contribute to various size and shape of particle which eventually affected the peak of surface plasmon resonance of the particles. Therefore, this research is aimed to get the optimum reaction pH and temperature in order to get the uniform nano size distribution of AgNPs. The resulting AgNPs were characterized by X-ray diffraction analysis, transmission electron microscope and UV-vis analysis. Result from UV-vis showed the absorbance peak was at ~430 nm which corresponding to silver nanoparticles with the morphological of the particle is quasi-spherical with the size is ~30 nm. Based on the result obtained, the result showed that the optimum temperature and reaction pH was achieved at 60 oC with the pH of 7, respectively. 2015 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/10697/1/Green%20Synthesis%20of%20Silver%20Nanoparticle-%20Effect%20of%20Reaction%20pH%20and%20Temperature.pdf Suriati, Ghazali and Nurul F., Salim (2015) Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature. In: International Conference on Chemistry and Chemical Engineering (ICCCE 2015), 14-15 May 2015 , Amsterdam, The Netherlands. .
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Suriati, Ghazali
Nurul F., Salim
Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
description Silver nanoparticles (AgNPs) is known as a particle of silver with size range is varied between 1 to 100 nm. Silver nanoparticles is widely use in biosensor and molecular labelling field. In the synthesis of AgNPs process, it is quite challenging to develop a controlled synthesis procedure in order to get the uniform nano size distribution. In this study, uniform and well-dispersed silver nanoparticles were prepared by a simple and green chemical reduction method. The particles were synthesized via the reduction of silver nitrate by the presence of glucose and ascorbic acid as reducing agent and surfactant, respectively. The reaction pH, temperature and time could contribute to various size and shape of particle which eventually affected the peak of surface plasmon resonance of the particles. Therefore, this research is aimed to get the optimum reaction pH and temperature in order to get the uniform nano size distribution of AgNPs. The resulting AgNPs were characterized by X-ray diffraction analysis, transmission electron microscope and UV-vis analysis. Result from UV-vis showed the absorbance peak was at ~430 nm which corresponding to silver nanoparticles with the morphological of the particle is quasi-spherical with the size is ~30 nm. Based on the result obtained, the result showed that the optimum temperature and reaction pH was achieved at 60 oC with the pH of 7, respectively.
format Conference or Workshop Item
author Suriati, Ghazali
Nurul F., Salim
author_facet Suriati, Ghazali
Nurul F., Salim
author_sort Suriati, Ghazali
title Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
title_short Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
title_full Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
title_fullStr Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
title_full_unstemmed Green Synthesis of Silver Nanoparticle: Effect of Reaction PH and Temperature
title_sort green synthesis of silver nanoparticle: effect of reaction ph and temperature
publishDate 2015
url http://umpir.ump.edu.my/id/eprint/10697/
http://umpir.ump.edu.my/id/eprint/10697/1/Green%20Synthesis%20of%20Silver%20Nanoparticle-%20Effect%20of%20Reaction%20pH%20and%20Temperature.pdf
first_indexed 2023-09-18T22:10:35Z
last_indexed 2023-09-18T22:10:35Z
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