Preparation of palm oil methyl esters for alkenyl succinic anhydride production

The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained...

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Main Authors: Nur Azreena Idris, Loh, Soh Kheang, Choo, Yuen May, Boey, Peng Lim
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2010
Online Access:http://journalarticle.ukm.my/7411/
http://journalarticle.ukm.my/7411/
http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf
id ukm-7411
recordtype eprints
spelling ukm-74112016-12-14T06:44:00Z http://journalarticle.ukm.my/7411/ Preparation of palm oil methyl esters for alkenyl succinic anhydride production Nur Azreena Idris, Loh, Soh Kheang Choo, Yuen May Boey, Peng Lim The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained via fractional distillation that separated the unsaturated fatty esters from the saturated fatty esters. The fractions with the highest content of unsaturated fatty esters were reacted with maleic anhydride (MA) for 8 hours at 240oC with the MA/FAME ratio of 1.5. The reaction was conducted without catalyst and solvent. The crude alkenyl succinic anhydride (ASA) obtained was purified by column chromatography. The purified compound was characterised by FTIR. Universiti Kebangsaan Malaysia 2010-10 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf Nur Azreena Idris, and Loh, Soh Kheang and Choo, Yuen May and Boey, Peng Lim (2010) Preparation of palm oil methyl esters for alkenyl succinic anhydride production. Sains Malaysiana, 39 (5). pp. 817-820. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num5_2010/contentsVol39num5_2010.html
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institution Universiti Kebangasaan Malaysia
building UKM Institutional Repository
collection Online Access
language English
description The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained via fractional distillation that separated the unsaturated fatty esters from the saturated fatty esters. The fractions with the highest content of unsaturated fatty esters were reacted with maleic anhydride (MA) for 8 hours at 240oC with the MA/FAME ratio of 1.5. The reaction was conducted without catalyst and solvent. The crude alkenyl succinic anhydride (ASA) obtained was purified by column chromatography. The purified compound was characterised by FTIR.
format Article
author Nur Azreena Idris,
Loh, Soh Kheang
Choo, Yuen May
Boey, Peng Lim
spellingShingle Nur Azreena Idris,
Loh, Soh Kheang
Choo, Yuen May
Boey, Peng Lim
Preparation of palm oil methyl esters for alkenyl succinic anhydride production
author_facet Nur Azreena Idris,
Loh, Soh Kheang
Choo, Yuen May
Boey, Peng Lim
author_sort Nur Azreena Idris,
title Preparation of palm oil methyl esters for alkenyl succinic anhydride production
title_short Preparation of palm oil methyl esters for alkenyl succinic anhydride production
title_full Preparation of palm oil methyl esters for alkenyl succinic anhydride production
title_fullStr Preparation of palm oil methyl esters for alkenyl succinic anhydride production
title_full_unstemmed Preparation of palm oil methyl esters for alkenyl succinic anhydride production
title_sort preparation of palm oil methyl esters for alkenyl succinic anhydride production
publisher Universiti Kebangsaan Malaysia
publishDate 2010
url http://journalarticle.ukm.my/7411/
http://journalarticle.ukm.my/7411/
http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf
first_indexed 2023-09-18T19:49:37Z
last_indexed 2023-09-18T19:49:37Z
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