A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry

A qualitative analysis of the individual compounds in Litsea fulva (locally known as ‘Medang’) essential oils was performed by comprehensive two-dimensional gas chromatography (GC × GC) coupled with time-of-flight mass spectrometer (TOF/MS) for the identification of the resolved peaks. Litsea fulva...

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Main Authors: Khong, Heng Yen, Laily Din, Zuriati Zakaria, Nor Hadiani Ismail, Nor Zamzurina Ismail, Mohd Ambar Yarmo
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2013
Online Access:http://journalarticle.ukm.my/6310/
http://journalarticle.ukm.my/6310/
http://journalarticle.ukm.my/6310/1/08_Khong_Heng_Yen.pdf
id ukm-6310
recordtype eprints
spelling ukm-63102016-12-14T06:40:49Z http://journalarticle.ukm.my/6310/ A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry Khong, Heng Yen Laily Din, Zuriati Zakaria, Nor Hadiani Ismail, Nor Zamzurina Ismail, Mohd Ambar Yarmo, A qualitative analysis of the individual compounds in Litsea fulva (locally known as ‘Medang’) essential oils was performed by comprehensive two-dimensional gas chromatography (GC × GC) coupled with time-of-flight mass spectrometer (TOF/MS) for the identification of the resolved peaks. Litsea fulva essential oil was found to contain 98 identifiable peaks with 32 compounds were identified with good matches. These compounds identified included 30 hydrocarbons, 22 alcohols, five acids, 16 ketones, five aldehydes, 12 esters, six ethers and two other compounds. The L. fulva leaf oil contained alcohols and ethers, with 34.09% and 24.38%, respectively. The major components of these oils were cis-Z-α-bisabolene epoxide (9.51%), trans-Z-α-bisabolene epoxide (8.36%), C13H20O2 (7.39%), longipinocarvone (5.68%), τ-Cadinol (4.24%), C15H24O (4.98%) and α-cadinol (3.95%). The study also showed that the comprehensive two-dimensional gas chromatography (GC × GC) is a better and more powerful separation tool in GC and an identification tool for analyzing complex volatile oils compared with the one-dimensional GC. Universiti Kebangsaan Malaysia 2013-07 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/6310/1/08_Khong_Heng_Yen.pdf Khong, Heng Yen and Laily Din, and Zuriati Zakaria, and Nor Hadiani Ismail, and Nor Zamzurina Ismail, and Mohd Ambar Yarmo, (2013) A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry. Sains Malaysiana, 42 (7). pp. 943-948. ISSN 0126-6039 http://www.ukm.my/jsm/
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institution Universiti Kebangasaan Malaysia
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language English
description A qualitative analysis of the individual compounds in Litsea fulva (locally known as ‘Medang’) essential oils was performed by comprehensive two-dimensional gas chromatography (GC × GC) coupled with time-of-flight mass spectrometer (TOF/MS) for the identification of the resolved peaks. Litsea fulva essential oil was found to contain 98 identifiable peaks with 32 compounds were identified with good matches. These compounds identified included 30 hydrocarbons, 22 alcohols, five acids, 16 ketones, five aldehydes, 12 esters, six ethers and two other compounds. The L. fulva leaf oil contained alcohols and ethers, with 34.09% and 24.38%, respectively. The major components of these oils were cis-Z-α-bisabolene epoxide (9.51%), trans-Z-α-bisabolene epoxide (8.36%), C13H20O2 (7.39%), longipinocarvone (5.68%), τ-Cadinol (4.24%), C15H24O (4.98%) and α-cadinol (3.95%). The study also showed that the comprehensive two-dimensional gas chromatography (GC × GC) is a better and more powerful separation tool in GC and an identification tool for analyzing complex volatile oils compared with the one-dimensional GC.
format Article
author Khong, Heng Yen
Laily Din,
Zuriati Zakaria,
Nor Hadiani Ismail,
Nor Zamzurina Ismail,
Mohd Ambar Yarmo,
spellingShingle Khong, Heng Yen
Laily Din,
Zuriati Zakaria,
Nor Hadiani Ismail,
Nor Zamzurina Ismail,
Mohd Ambar Yarmo,
A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
author_facet Khong, Heng Yen
Laily Din,
Zuriati Zakaria,
Nor Hadiani Ismail,
Nor Zamzurina Ismail,
Mohd Ambar Yarmo,
author_sort Khong, Heng Yen
title A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
title_short A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
title_full A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
title_fullStr A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
title_full_unstemmed A qualitative analysis of Litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
title_sort qualitative analysis of litsea fulva essential oils using comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry
publisher Universiti Kebangsaan Malaysia
publishDate 2013
url http://journalarticle.ukm.my/6310/
http://journalarticle.ukm.my/6310/
http://journalarticle.ukm.my/6310/1/08_Khong_Heng_Yen.pdf
first_indexed 2023-09-18T19:46:33Z
last_indexed 2023-09-18T19:46:33Z
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