Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time

This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis...

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Main Authors:	Nik Roselina, N.R, Azizan, A, Lockman, Z
Format:	Article
Language:	English
Published:	Universiti Kebangsaan Malaysia 2012
Online Access:	http://journalarticle.ukm.my/5427/ http://journalarticle.ukm.my/5427/ http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf

id	ukm-5427
recordtype	eprints
spelling	ukm-54272016-12-14T06:38:25Z http://journalarticle.ukm.my/5427/ Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time Nik Roselina, N.R Azizan, A Lockman, Z This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis also indicated that the as-synthesized nanoparticles were pure Ni with face-centered cubic (fcc) crystal structure. Transmission electron microscopy (TEM) results showed that the sample with heating duration of 15 min has the most narrow size distribution and the size increased as the reaction time increased. Universiti Kebangsaan Malaysia 2012-08 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf Nik Roselina, N.R and Azizan, A and Lockman, Z (2012) Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time. Sains Malaysiana, 41 (8). pp. 1037-1042. ISSN 0126-6039 http://www.ukm.my/jsm/
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis also indicated that the as-synthesized nanoparticles were pure Ni with face-centered cubic (fcc) crystal structure. Transmission electron microscopy (TEM) results showed that the sample with heating duration of 15 min has the most narrow size distribution and the size increased as the reaction time increased.
format	Article
author	Nik Roselina, N.R Azizan, A Lockman, Z
spellingShingle	Nik Roselina, N.R Azizan, A Lockman, Z Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
author_facet	Nik Roselina, N.R Azizan, A Lockman, Z
author_sort	Nik Roselina, N.R
title	Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_short	Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_full	Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_fullStr	Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_full_unstemmed	Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_sort	synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
publisher	Universiti Kebangsaan Malaysia
publishDate	2012
url	http://journalarticle.ukm.my/5427/ http://journalarticle.ukm.my/5427/ http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf
first_indexed	2023-09-18T19:44:07Z
last_indexed	2023-09-18T19:44:07Z
_version_	1777405785790218240

Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time

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