Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films

The aim of this project was to investigate the effect of ZnO addition on the structural properties of ZnO-PANi/carbon black thin films. The sol gel method was employed for the preparation of ZnO sol. The sol was dried for 24 h at 100°C and then annealed at 600°C for 5 h. XRD characterization of the...

Full description

Bibliographic Details
Main Authors:	Siti Fariza Mat Tahir, Norhashimah Ramli, Izura Izzuddin, Muhamad Mat Salleh, Muhammad Yahaya, Akrajas Ali Umar, Mohammad Hafizuddin Haji Jumali
Format:	Article
Language:	English
Published:	Universiti Kebangsaan Malaysia 2012
Online Access:	http://journalarticle.ukm.my/5421/ http://journalarticle.ukm.my/5421/ http://journalarticle.ukm.my/5421/1/09%2520siti%2520fariza.pdf

id	ukm-5421
recordtype	eprints
spelling	ukm-54212016-12-14T06:38:24Z http://journalarticle.ukm.my/5421/ Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films Siti Fariza Mat Tahir, Norhashimah Ramli, Izura Izzuddin, Muhamad Mat Salleh, Muhammad Yahaya, Akrajas Ali Umar, Mohammad Hafizuddin Haji Jumali, The aim of this project was to investigate the effect of ZnO addition on the structural properties of ZnO-PANi/carbon black thin films. The sol gel method was employed for the preparation of ZnO sol. The sol was dried for 24 h at 100°C and then annealed at 600°C for 5 h. XRD characterization of the ZnO powder showed the formation of wurtzite type ZnO crystals. The ZnO powder were mixed into PANi/carbon black solution which was dissolved into M-Pyrol, N-Methyl-2-Pyrrolidinone (NMP) to produce a composite solution of ZnO-PANi/carbon black. The weight ratio of ZnO were 4 wt%, 6 wt% and 8 wt%. The composite solutions were deposited onto glass substrates using a spin-coating technique to fabricate ZnO-PANi/carbon black thin films. AFM characterization showed the decreasing of average roughness from 7.98 nm to 2.23 nm with the increment of ZnO addition in PANi/carbon black films. The thickness of the films also decreased from 59.5 nm to 28.3 nm. FESEM image revealed that ZnO-PANi/carbon black thin films have changed into agglomerated surface morphology resulting in the increment of porosity of the films. Universiti Kebangsaan Malaysia 2012-08 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/5421/1/09%2520siti%2520fariza.pdf Siti Fariza Mat Tahir, and Norhashimah Ramli, and Izura Izzuddin, and Muhamad Mat Salleh, and Muhammad Yahaya, and Akrajas Ali Umar, and Mohammad Hafizuddin Haji Jumali, (2012) Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films. Sains Malaysiana, 41 (8). pp. 1001-1004. ISSN 0126-6039 http://www.ukm.my/jsm/
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	The aim of this project was to investigate the effect of ZnO addition on the structural properties of ZnO-PANi/carbon black thin films. The sol gel method was employed for the preparation of ZnO sol. The sol was dried for 24 h at 100°C and then annealed at 600°C for 5 h. XRD characterization of the ZnO powder showed the formation of wurtzite type ZnO crystals. The ZnO powder were mixed into PANi/carbon black solution which was dissolved into M-Pyrol, N-Methyl-2-Pyrrolidinone (NMP) to produce a composite solution of ZnO-PANi/carbon black. The weight ratio of ZnO were 4 wt%, 6 wt% and 8 wt%. The composite solutions were deposited onto glass substrates using a spin-coating technique to fabricate ZnO-PANi/carbon black thin films. AFM characterization showed the decreasing of average roughness from 7.98 nm to 2.23 nm with the increment of ZnO addition in PANi/carbon black films. The thickness of the films also decreased from 59.5 nm to 28.3 nm. FESEM image revealed that ZnO-PANi/carbon black thin films have changed into agglomerated surface morphology resulting in the increment of porosity of the films.
format	Article
author	Siti Fariza Mat Tahir, Norhashimah Ramli, Izura Izzuddin, Muhamad Mat Salleh, Muhammad Yahaya, Akrajas Ali Umar, Mohammad Hafizuddin Haji Jumali,
spellingShingle	Siti Fariza Mat Tahir, Norhashimah Ramli, Izura Izzuddin, Muhamad Mat Salleh, Muhammad Yahaya, Akrajas Ali Umar, Mohammad Hafizuddin Haji Jumali, Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
author_facet	Siti Fariza Mat Tahir, Norhashimah Ramli, Izura Izzuddin, Muhamad Mat Salleh, Muhammad Yahaya, Akrajas Ali Umar, Mohammad Hafizuddin Haji Jumali,
author_sort	Siti Fariza Mat Tahir,
title	Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
title_short	Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
title_full	Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
title_fullStr	Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
title_full_unstemmed	Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films
title_sort	effect of zno addition on structural properties of zno-pani/carbon black thin films
publisher	Universiti Kebangsaan Malaysia
publishDate	2012
url	http://journalarticle.ukm.my/5421/ http://journalarticle.ukm.my/5421/ http://journalarticle.ukm.my/5421/1/09%2520siti%2520fariza.pdf
first_indexed	2023-09-18T19:44:06Z
last_indexed	2023-09-18T19:44:06Z
_version_	1777405784914657280

Effect of ZnO addition on structural properties of ZnO-PANi/carbon black thin films

Similar Items