Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system

The effect of composition on nickel cobaltites prepared by co-precipitation was investigated. Various compositions were synthesised under different heat treatment conditions. The formation mechanism, lattice parameter and crystallite size were determined by various techniques. X-ray dffraction (XR...

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Main Authors:	Chang, Sook-Keng, Zulkarnain Zainal, Tan, Kar-Ban, Nor Azah Yusof
Format:	Article
Language:	English
Published:	Universiti Kebangsaan Malaysia 2012
Online Access:	http://journalarticle.ukm.my/3937/ http://journalarticle.ukm.my/3937/ http://journalarticle.ukm.my/3937/1/12%2520Sook-keng.pdf

id	ukm-3937
recordtype	eprints
spelling	ukm-39372016-12-14T06:35:22Z http://journalarticle.ukm.my/3937/ Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system Chang, Sook-Keng Zulkarnain Zainal, Tan, Kar-Ban Nor Azah Yusof, The effect of composition on nickel cobaltites prepared by co-precipitation was investigated. Various compositions were synthesised under different heat treatment conditions. The formation mechanism, lattice parameter and crystallite size were determined by various techniques. X-ray dffraction (XRD) analysis revealed that the optimum condition for the formation of single phase nickel-cobalt oxide (NiCo2O4) can be obtained from solution containing Ni: Co ratio of 33.3 mol%: 66.7 mol% with heat treatment at 400 °C. The presence of pure phase NiCo2O4 with the particle size of approximately 34.10 nm was also observed in field emission scanning electron microscopy (FESEM). The crystallinity of the synthesized oxides was improved with the increment of Ni content. Universiti Kebangsaan Malaysia 2012-04 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/3937/1/12%2520Sook-keng.pdf Chang, Sook-Keng and Zulkarnain Zainal, and Tan, Kar-Ban and Nor Azah Yusof, (2012) Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system. Sains Malaysiana, 41 (4). pp. 465-470. ISSN 0126-6039 http://www.ukm.my/jsm
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	The effect of composition on nickel cobaltites prepared by co-precipitation was investigated. Various compositions were synthesised under different heat treatment conditions. The formation mechanism, lattice parameter and crystallite size were determined by various techniques. X-ray dffraction (XRD) analysis revealed that the optimum condition for the formation of single phase nickel-cobalt oxide (NiCo2O4) can be obtained from solution containing Ni: Co ratio of 33.3 mol%: 66.7 mol% with heat treatment at 400 °C. The presence of pure phase NiCo2O4 with the particle size of approximately 34.10 nm was also observed in field emission scanning electron microscopy (FESEM). The crystallinity of the synthesized oxides was improved with the increment of Ni content.
format	Article
author	Chang, Sook-Keng Zulkarnain Zainal, Tan, Kar-Ban Nor Azah Yusof,
spellingShingle	Chang, Sook-Keng Zulkarnain Zainal, Tan, Kar-Ban Nor Azah Yusof, Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
author_facet	Chang, Sook-Keng Zulkarnain Zainal, Tan, Kar-Ban Nor Azah Yusof,
author_sort	Chang, Sook-Keng
title	Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
title_short	Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
title_full	Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
title_fullStr	Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
title_full_unstemmed	Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
title_sort	surface morphology and crystallinity of metal oxides in nickel-cobalt binary system
publisher	Universiti Kebangsaan Malaysia
publishDate	2012
url	http://journalarticle.ukm.my/3937/ http://journalarticle.ukm.my/3937/ http://journalarticle.ukm.my/3937/1/12%2520Sook-keng.pdf
first_indexed	2023-09-18T19:40:10Z
last_indexed	2023-09-18T19:40:10Z
_version_	1777405536612909056

Surface morphology and crystallinity of metal oxides in nickel-cobalt binary system

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