Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak

Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9- fluorenecarboxylate was successfully accomplished by self assembly method with molar ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate ranging from 0.2 M to 0.8 M . The pH of the synthesi...

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Main Author: Abdul Razak, Mohd Hafiz
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2009
Online Access:http://ir.uitm.edu.my/id/eprint/756/
http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf
id uitm-756
recordtype eprints
spelling uitm-7562017-04-21T06:11:46Z http://ir.uitm.edu.my/id/eprint/756/ Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak Abdul Razak, Mohd Hafiz Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9- fluorenecarboxylate was successfully accomplished by self assembly method with molar ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate ranging from 0.2 M to 0.8 M . The pH of the synthesis was kept constant at 7.5. As a result of the successful intercalation of 9-hydroxy-9-fluorenecarboxylate anion into zincaluminium- layered double hydroxide, an expansion of the interlayer spacing from 8.9 Å in the layered double hydroxide to 14.3 Å in the zinc-aluminium9-hydroxy-9- fluorenecarboxylate nanocomposite could be observed in the PXRD diffractogram. The percentage loading of the guest anion, 9-hydroxy-9-fluorenecarboxylate in the layered double hydroxide was estimated to be about 76-78% (w/w) at the optimum condition Faculty of Applied Sciences 2009 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf Abdul Razak, Mohd Hafiz (2009) Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak. [Student Project] (Unpublished)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
description Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9- fluorenecarboxylate was successfully accomplished by self assembly method with molar ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate ranging from 0.2 M to 0.8 M . The pH of the synthesis was kept constant at 7.5. As a result of the successful intercalation of 9-hydroxy-9-fluorenecarboxylate anion into zincaluminium- layered double hydroxide, an expansion of the interlayer spacing from 8.9 Å in the layered double hydroxide to 14.3 Å in the zinc-aluminium9-hydroxy-9- fluorenecarboxylate nanocomposite could be observed in the PXRD diffractogram. The percentage loading of the guest anion, 9-hydroxy-9-fluorenecarboxylate in the layered double hydroxide was estimated to be about 76-78% (w/w) at the optimum condition
format Student Project
author Abdul Razak, Mohd Hafiz
spellingShingle Abdul Razak, Mohd Hafiz
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
author_facet Abdul Razak, Mohd Hafiz
author_sort Abdul Razak, Mohd Hafiz
title Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
title_short Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
title_full Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
title_fullStr Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
title_full_unstemmed Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
title_sort synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / mohd hafiz abdul razak
publisher Faculty of Applied Sciences
publishDate 2009
url http://ir.uitm.edu.my/id/eprint/756/
http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf
first_indexed 2023-09-18T22:44:59Z
last_indexed 2023-09-18T22:44:59Z
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