Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid
Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) a...
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Faculty of Applied Sciences
2017
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| Online Access: | http://ir.uitm.edu.my/id/eprint/25362/ http://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf |
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eprints |
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uitm-253622019-09-11T02:32:31Z http://ir.uitm.edu.my/id/eprint/25362/ Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid Rashid, Shuhaili QD Chemistry Oxidation Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD) analysis. MNPs coated PANI (MNPs/PANI) showed higher capabilities to remove 2,4- dinitrophenol (2.4-DNP) via spectrophotometry at 358 nm by using Ultraviolet Visible (UV-Vis) Spectrophotometer. Different parameters such as pH, contact time, initial concentration and temperature, amount of adsorbent, interfering ions were investigated to optimize the performance of MNPs/P ANI in removal of 2,4-DNP. In addition, the reusabilities of MNPs/P ANI was also studied to add up its economic value. The best perfonnance of MNPs/P ANI to remove 2,4-DNP molecules was found at pH 7, I 05 minutes contact time, IO ppm initial concentration of 2,4-DNP with 298.15 K temperature and I 0 mg of adsorbent amount. The percentage removal (¾R) of 2,4-DNP was still up to 90% in the presence of chloride (Cl-) ions, nitrate (NO3-) ions and sulfate (SO42-) ions. Lastly MNPs/P ANI was used up to five cycles. Faculty of Applied Sciences 2017 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf Rashid, Shuhaili (2017) Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid. [Student Project] (Unpublished) |
| repository_type |
Digital Repository |
| institution_category |
Local University |
| institution |
Universiti Teknologi MARA |
| building |
UiTM Institutional Repository |
| collection |
Online Access |
| language |
English |
| topic |
QD Chemistry Oxidation |
| spellingShingle |
QD Chemistry Oxidation Rashid, Shuhaili Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| description |
Magnetic nanoparticles ( MNPs) coated polyaniline (P ANI) was successfully synthesized and further used for removal of 2.4-dinitrophenol. The presence of PANI coatings on the surface of MNPs was confirmed by using Fourier Transform
Infrared (FT-IR) Spectroscopy. Scanning Electron Microscopy (SEM) and X-ray Diffractometry (XRD) analysis. MNPs coated PANI (MNPs/PANI) showed higher capabilities to remove 2,4- dinitrophenol (2.4-DNP) via spectrophotometry at 358 nm by using Ultraviolet Visible (UV-Vis) Spectrophotometer. Different parameters
such as pH, contact time, initial concentration and temperature, amount of adsorbent, interfering ions were investigated to optimize the performance of MNPs/P ANI in removal of 2,4-DNP. In addition, the reusabilities of MNPs/P ANI was also studied to add up its economic value. The best perfonnance of
MNPs/P ANI to remove 2,4-DNP molecules was found at pH 7, I 05 minutes contact time, IO ppm initial concentration of 2,4-DNP with 298.15 K temperature and I 0 mg of adsorbent amount. The percentage removal (¾R) of 2,4-DNP was still up to 90% in the presence of chloride (Cl-) ions, nitrate (NO3-) ions and sulfate (SO42-)
ions. Lastly MNPs/P ANI was used up to five cycles. |
| format |
Student Project |
| author |
Rashid, Shuhaili |
| author_facet |
Rashid, Shuhaili |
| author_sort |
Rashid, Shuhaili |
| title |
Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_short |
Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_full |
Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_fullStr |
Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_full_unstemmed |
Synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / Shuhaili Rashid |
| title_sort |
synthesis and characterization of magnetic nanoparticles coated with poly aniline for removal of 2,4-dinitrophenol / shuhaili rashid |
| publisher |
Faculty of Applied Sciences |
| publishDate |
2017 |
| url |
http://ir.uitm.edu.my/id/eprint/25362/ http://ir.uitm.edu.my/id/eprint/25362/1/PPb_SHUHAILI%20RASHID%20AS%20N%2017_5.pdf |
| first_indexed |
2023-09-18T23:14:35Z |
| last_indexed |
2023-09-18T23:14:35Z |
| _version_ |
1777419026685755392 |