Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan

A Schiff base ligand derived from 5-bromosalicylaldehyde and ethylenediamine undergo further insertion with transition metal namely, Mn(II) and Cu(II) were synthesized and characterized by using melting point determination, molar conductivity measurements, elemental analysis (CHNS), IR and UV-Vis sp...

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Main Author: Norzaini Tan, Nur Azirah
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2016
Subjects:
Online Access:http://ir.uitm.edu.my/id/eprint/24533/
http://ir.uitm.edu.my/id/eprint/24533/1/PPb_NUR%20AZIRAH%20NORZAINI%20TAN%20AS%20N%2016_5.pdf
id uitm-24533
recordtype eprints
spelling uitm-245332019-07-19T00:34:37Z http://ir.uitm.edu.my/id/eprint/24533/ Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan Norzaini Tan, Nur Azirah Schiff bases Metal complexes. Layered double hydroxides A Schiff base ligand derived from 5-bromosalicylaldehyde and ethylenediamine undergo further insertion with transition metal namely, Mn(II) and Cu(II) were synthesized and characterized by using melting point determination, molar conductivity measurements, elemental analysis (CHNS), IR and UV-Vis spectroscopy. The results obtained shows that the ligand behaves as a tetradentate ligand coordinate through azomethine nitrogen and phenolic oxygen, produces tetrahedral and an octahedral geometry for Mn(II) and Cu(II) complexes, respectively. The synthesized compounds were tested against anti-corrosion activity where they shows an appreciable corrosion inhibition efficiency against the corrosion of mild steel in 1 M HCl solution at 40 °C. It have been found that MnL shows a greater corrosion inhibition efficiency than L and CuL. As the concentration of studied inhibitors increases, the corrosion inhibition efficiency of the prepared compounds also increases. Faculty of Applied Sciences 2016 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/24533/1/PPb_NUR%20AZIRAH%20NORZAINI%20TAN%20AS%20N%2016_5.pdf Norzaini Tan, Nur Azirah (2016) Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan. [Student Project] (Submitted)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic Schiff bases
Metal complexes. Layered double hydroxides
spellingShingle Schiff bases
Metal complexes. Layered double hydroxides
Norzaini Tan, Nur Azirah
Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
description A Schiff base ligand derived from 5-bromosalicylaldehyde and ethylenediamine undergo further insertion with transition metal namely, Mn(II) and Cu(II) were synthesized and characterized by using melting point determination, molar conductivity measurements, elemental analysis (CHNS), IR and UV-Vis spectroscopy. The results obtained shows that the ligand behaves as a tetradentate ligand coordinate through azomethine nitrogen and phenolic oxygen, produces tetrahedral and an octahedral geometry for Mn(II) and Cu(II) complexes, respectively. The synthesized compounds were tested against anti-corrosion activity where they shows an appreciable corrosion inhibition efficiency against the corrosion of mild steel in 1 M HCl solution at 40 °C. It have been found that MnL shows a greater corrosion inhibition efficiency than L and CuL. As the concentration of studied inhibitors increases, the corrosion inhibition efficiency of the prepared compounds also increases.
format Student Project
author Norzaini Tan, Nur Azirah
author_facet Norzaini Tan, Nur Azirah
author_sort Norzaini Tan, Nur Azirah
title Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
title_short Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
title_full Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
title_fullStr Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
title_full_unstemmed Synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / Nur Azirah Norzaini Tan
title_sort synthesis, characterization and anti-corrosion screening of schiff base ligand and its metal complexes / nur azirah norzaini tan
publisher Faculty of Applied Sciences
publishDate 2016
url http://ir.uitm.edu.my/id/eprint/24533/
http://ir.uitm.edu.my/id/eprint/24533/1/PPb_NUR%20AZIRAH%20NORZAINI%20TAN%20AS%20N%2016_5.pdf
first_indexed 2023-09-18T23:12:47Z
last_indexed 2023-09-18T23:12:47Z
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