Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan

Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan

Two Schiff base ligand has been synthesized by the condensation of salicylaldehyde with aniline and 1,2-diaminocyclohexane which produced p-benzalaminophenol [SBl] and N,N'-bis(salicylidene)cyclohexanediamine [SB2] respectively. The ligands were further synthesized with manganese (II) acetate w...

Full description

Bibliographic Details
Main Author: Roslan, Norhafiza
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2010
Subjects:
Schiff bases
Online Access:http://ir.uitm.edu.my/id/eprint/23095/
http://ir.uitm.edu.my/id/eprint/23095/1/PPb_NORHAFIZA%20ROSLAN%20AS%2010_5.pdf
id uitm-23095
recordtype eprints
spelling uitm-230952019-02-27T07:53:57Z http://ir.uitm.edu.my/id/eprint/23095/ Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan Roslan, Norhafiza Schiff bases Two Schiff base ligand has been synthesized by the condensation of salicylaldehyde with aniline and 1,2-diaminocyclohexane which produced p-benzalaminophenol [SBl] and N,N'-bis(salicylidene)cyclohexanediamine [SB2] respectively. The ligands were further synthesized with manganese (II) acetate which produced [Mn(II){SBl}] and [Mn(II){SB2}] complexes. These ligands and complexes were then characterized by elemental CHN analysis, FTIR, UV-Vis, ¹H-NMR and ¹³C-NMR spectroscopies. FTIR, UV-Vis, ¹H-NMR and ¹³C-NMR spectroscopic data revealed that the ligands acted as bidentate ligand for [SBl] and tetradentate ligand for [SB2]. While FTIR and UV-Vis spectroscopic data showed that the ligands from [SBl] and [SB2] were coordinated to Mn atom through both the azomethine N atoms and phenolic O atoms to become as their complexes. Faculty of Applied Sciences 2010 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/23095/1/PPb_NORHAFIZA%20ROSLAN%20AS%2010_5.pdf Roslan, Norhafiza (2010) Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan. [Student Project] (Unpublished)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic Schiff bases
spellingShingle Schiff bases
Roslan, Norhafiza
Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
description Two Schiff base ligand has been synthesized by the condensation of salicylaldehyde with aniline and 1,2-diaminocyclohexane which produced p-benzalaminophenol [SBl] and N,N'-bis(salicylidene)cyclohexanediamine [SB2] respectively. The ligands were further synthesized with manganese (II) acetate which produced [Mn(II){SBl}] and [Mn(II){SB2}] complexes. These ligands and complexes were then characterized by elemental CHN analysis, FTIR, UV-Vis, ¹H-NMR and ¹³C-NMR spectroscopies. FTIR, UV-Vis, ¹H-NMR and ¹³C-NMR spectroscopic data revealed that the ligands acted as bidentate ligand for [SBl] and tetradentate ligand for [SB2]. While FTIR and UV-Vis spectroscopic data showed that the ligands from [SBl] and [SB2] were coordinated to Mn atom through both the azomethine N atoms and phenolic O atoms to become as their complexes.
format Student Project
author Roslan, Norhafiza
author_facet Roslan, Norhafiza
author_sort Roslan, Norhafiza
title Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
title_short Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
title_full Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
title_fullStr Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
title_full_unstemmed Synthesis and characterization of manganese (II) complexes with N, O- donor schiff base / Norhafiza Roslan
title_sort synthesis and characterization of manganese (ii) complexes with n, o- donor schiff base / norhafiza roslan
publisher Faculty of Applied Sciences
publishDate 2010
url http://ir.uitm.edu.my/id/eprint/23095/
http://ir.uitm.edu.my/id/eprint/23095/1/PPb_NORHAFIZA%20ROSLAN%20AS%2010_5.pdf
first_indexed 2023-09-18T23:10:02Z
last_indexed 2023-09-18T23:10:02Z
_version_ 1777418741192065024

Similar Items