Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]

In this study, Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) was prepared by acetic acid-assisted sol-gel method The structural properties of NASICON phosphates material with chemical formula LiTi₂(P0₄)₃ were observed using the Fourier transform infrared spectroscopy. NASICON is a family of crystallin...

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Main Authors:	Hamidi, Maziidah, Mohamed, S. N., Raja Mustapha, Raja Ibrahim Puter, Hassan, Oskar Hasdinor, Yahya, Muhd Zu Azhan
Format:	Article
Language:	English
Published:	Institute of Research Management and Innovation (IRMI) 2015
Subjects:	Physical and theoretical chemistry
Online Access:	http://ir.uitm.edu.my/id/eprint/16083/ http://ir.uitm.edu.my/id/eprint/16083/1/AJ_MAZIIDAH%20HAMIDI%20SRJ%2015.pdf

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recordtype	eprints
spelling	uitm-160832017-02-02T07:44:29Z http://ir.uitm.edu.my/id/eprint/16083/ Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.] Hamidi, Maziidah Mohamed, S. N. Raja Mustapha, Raja Ibrahim Puter Hassan, Oskar Hasdinor Yahya, Muhd Zu Azhan Physical and theoretical chemistry In this study, Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) was prepared by acetic acid-assisted sol-gel method The structural properties of NASICON phosphates material with chemical formula LiTi₂(P0₄)₃ were observed using the Fourier transform infrared spectroscopy. NASICON is a family of crystalline phosphate with a general network system consisting of P0₄ tetrahedra, thus bands were assigned by vibrations contributed by basic phosphates, in the wavenumber region between 1300 cm1 and 600 cm1. Experimental spectra indicated that all Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5), heat treated at 600°C and 700°Cfor 3 hours in air, samples showed the presence of phosphate peaks with shift in frequency asAl3⁺ is substituted into the structure, and with increasing temperatures. Some bands broadened and overlapped causing it hard to analyze the arising bands. It however determined the existence of NASICON structure in all of the samples under study. Institute of Research Management and Innovation (IRMI) 2015 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/16083/1/AJ_MAZIIDAH%20HAMIDI%20SRJ%2015.pdf Hamidi, Maziidah and Mohamed, S. N. and Raja Mustapha, Raja Ibrahim Puter and Hassan, Oskar Hasdinor and Yahya, Muhd Zu Azhan (2015) Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]. Scientific Research Journal, 12 (2). pp. 36-44. ISSN 1675-7009
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Teknologi MARA
building	UiTM Institutional Repository
collection	Online Access
language	English
topic	Physical and theoretical chemistry
spellingShingle	Physical and theoretical chemistry Hamidi, Maziidah Mohamed, S. N. Raja Mustapha, Raja Ibrahim Puter Hassan, Oskar Hasdinor Yahya, Muhd Zu Azhan Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
description	In this study, Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) was prepared by acetic acid-assisted sol-gel method The structural properties of NASICON phosphates material with chemical formula LiTi₂(P0₄)₃ were observed using the Fourier transform infrared spectroscopy. NASICON is a family of crystalline phosphate with a general network system consisting of P0₄ tetrahedra, thus bands were assigned by vibrations contributed by basic phosphates, in the wavenumber region between 1300 cm1 and 600 cm1. Experimental spectra indicated that all Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5), heat treated at 600°C and 700°Cfor 3 hours in air, samples showed the presence of phosphate peaks with shift in frequency asAl3⁺ is substituted into the structure, and with increasing temperatures. Some bands broadened and overlapped causing it hard to analyze the arising bands. It however determined the existence of NASICON structure in all of the samples under study.
format	Article
author	Hamidi, Maziidah Mohamed, S. N. Raja Mustapha, Raja Ibrahim Puter Hassan, Oskar Hasdinor Yahya, Muhd Zu Azhan
author_facet	Hamidi, Maziidah Mohamed, S. N. Raja Mustapha, Raja Ibrahim Puter Hassan, Oskar Hasdinor Yahya, Muhd Zu Azhan
author_sort	Hamidi, Maziidah
title	Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
title_short	Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
title_full	Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
title_fullStr	Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
title_full_unstemmed	Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]
title_sort	vibrational analysis of li₁₊ₓalₓti₂₋ₓ(p0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / maziidah hamidi … [et al.]
publisher	Institute of Research Management and Innovation (IRMI)
publishDate	2015
url	http://ir.uitm.edu.my/id/eprint/16083/ http://ir.uitm.edu.my/id/eprint/16083/1/AJ_MAZIIDAH%20HAMIDI%20SRJ%2015.pdf
first_indexed	2023-09-18T22:55:18Z
last_indexed	2023-09-18T22:55:18Z
_version_	1777417813999222784

Vibrational analysis of Li₁₊ₓAlₓTi₂₋ₓ(P0₄)₃ (0.0 < x < 0.5) glass ceramic electrolytes prepared by acetic acid-assisted sol-gel method / Maziidah Hamidi … [et al.]

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