Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]

The TiO2 photocatalyst is used for various purposes such as a cleanup of polluted air, antifouling, sterilization, deodorization, and so on. The purpose of this study is to synthesize the TiO2 photocatalyst fines in the gas phase. We used TTIP (titanium tetraisopropoxide) as the precursor because g...

Full description

Bibliographic Details
Main Authors: Mameda, Ayumi, Shioi, Masahiko, Sakai, Yuka, Ito, Takuya, Kato, Shigeru, Yamasaki, Akihiro, Suzuki, Seiichi, Kojima, Toshinori
Format: Article
Language:English
Published: Universiti Teknologi MARA, Pulau Pinang 2015
Subjects:
Online Access:http://ir.uitm.edu.my/id/eprint/11985/
http://ir.uitm.edu.my/id/eprint/11985/1/AJ_AYUMI%20MAMEDA%20EAJ%2015.pdf
id uitm-11985
recordtype eprints
spelling uitm-119852016-07-20T03:05:36Z http://ir.uitm.edu.my/id/eprint/11985/ Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.] Mameda, Ayumi Shioi, Masahiko Sakai, Yuka Ito, Takuya Kato, Shigeru Yamasaki, Akihiro Suzuki, Seiichi Kojima, Toshinori QD Chemistry Gas as fuel Gas industry The TiO2 photocatalyst is used for various purposes such as a cleanup of polluted air, antifouling, sterilization, deodorization, and so on. The purpose of this study is to synthesize the TiO2 photocatalyst fines in the gas phase. We used TTIP (titanium tetraisopropoxide) as the precursor because gas phase processes using chlorine compounds cause serious operational problems such as corrosion. As TTIP has close boiling and thermal decomposition temperatures, liquid TTIP was directly (without vaporization) introduced through a water-cooled tube, while, H2O vaporized in a separate vaporizer was introduced from the lower part of the reactor. At the reactor temperature of 1000oC, the more Ar flow rate at the TTIP side increased without changing the flow rate of TTIP keeping the total flow rates of TTIP side and H2O side almost similar, the smaller particle size of TiO2 was elaborated, the less the carbon content became, and the higher photocatalytic activity was observed. Then, the effect of reactor temperature between 800oC and 1100oC was examined under the optimum condition of flow rate. At the reactor temperature of 1000oC, small particle size of TiO2 with the highest anatase content was elaborated, which showed the highest photocatalytic activity. Universiti Teknologi MARA, Pulau Pinang 2015 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/11985/1/AJ_AYUMI%20MAMEDA%20EAJ%2015.pdf Mameda, Ayumi and Shioi, Masahiko and Sakai, Yuka and Ito, Takuya and Kato, Shigeru and Yamasaki, Akihiro and Suzuki, Seiichi and Kojima, Toshinori (2015) Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]. Esteem Academic Journal, 11 (1). pp. 44-53. ISSN 1675-7939
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic QD Chemistry
Gas as fuel
Gas industry
spellingShingle QD Chemistry
Gas as fuel
Gas industry
Mameda, Ayumi
Shioi, Masahiko
Sakai, Yuka
Ito, Takuya
Kato, Shigeru
Yamasaki, Akihiro
Suzuki, Seiichi
Kojima, Toshinori
Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
description The TiO2 photocatalyst is used for various purposes such as a cleanup of polluted air, antifouling, sterilization, deodorization, and so on. The purpose of this study is to synthesize the TiO2 photocatalyst fines in the gas phase. We used TTIP (titanium tetraisopropoxide) as the precursor because gas phase processes using chlorine compounds cause serious operational problems such as corrosion. As TTIP has close boiling and thermal decomposition temperatures, liquid TTIP was directly (without vaporization) introduced through a water-cooled tube, while, H2O vaporized in a separate vaporizer was introduced from the lower part of the reactor. At the reactor temperature of 1000oC, the more Ar flow rate at the TTIP side increased without changing the flow rate of TTIP keeping the total flow rates of TTIP side and H2O side almost similar, the smaller particle size of TiO2 was elaborated, the less the carbon content became, and the higher photocatalytic activity was observed. Then, the effect of reactor temperature between 800oC and 1100oC was examined under the optimum condition of flow rate. At the reactor temperature of 1000oC, small particle size of TiO2 with the highest anatase content was elaborated, which showed the highest photocatalytic activity.
format Article
author Mameda, Ayumi
Shioi, Masahiko
Sakai, Yuka
Ito, Takuya
Kato, Shigeru
Yamasaki, Akihiro
Suzuki, Seiichi
Kojima, Toshinori
author_facet Mameda, Ayumi
Shioi, Masahiko
Sakai, Yuka
Ito, Takuya
Kato, Shigeru
Yamasaki, Akihiro
Suzuki, Seiichi
Kojima, Toshinori
author_sort Mameda, Ayumi
title Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
title_short Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
title_full Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
title_fullStr Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
title_full_unstemmed Elaboration of photoactive tio particles by CVD : effect of operational parameters / Ayumi Mameda ... [et al.]
title_sort elaboration of photoactive tio particles by cvd : effect of operational parameters / ayumi mameda ... [et al.]
publisher Universiti Teknologi MARA, Pulau Pinang
publishDate 2015
url http://ir.uitm.edu.my/id/eprint/11985/
http://ir.uitm.edu.my/id/eprint/11985/1/AJ_AYUMI%20MAMEDA%20EAJ%2015.pdf
first_indexed 2023-09-18T22:48:48Z
last_indexed 2023-09-18T22:48:48Z
_version_ 1777417404495691776