The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.

Salacca zalacca (Gaertn.) Voss (salak fruit or snake fruit) is a species of palm tree native to Southwest Java and North Sumatra in Indonesia. It is known as one of the tropical fruits in Malaysia. It is a reddish-brown scaly skin with pleasant pineapple, pear and banana-like aromas. Its strong plea...

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Main Authors: Hilmi, Nur Nadhirah, Mat So'ad, Siti Zaiton, Siddiqui, Mohammad Jamshed Ahmad, Sarker, Md. Zaidul Islam, Rahman, Md. Mokhlesur, Juahir, Hafizan, Raja Hussin, Tengku Mohammad Ariff, Wan Nik, Wan Mohd Norsani, Siddique, Md Nurul Islam
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Language:English
English
English
English
Published: Oriental Scientific Publishing Company 2019
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spelling iium-769622020-01-02T02:52:20Z http://irep.iium.edu.my/76962/ The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss. Hilmi, Nur Nadhirah Mat So'ad, Siti Zaiton Siddiqui, Mohammad Jamshed Ahmad Sarker, Md. Zaidul Islam Rahman, Md. Mokhlesur Juahir, Hafizan Raja Hussin, Tengku Mohammad Ariff Wan Nik, Wan Mohd Norsani Siddique, Md Nurul Islam QD Chemistry Salacca zalacca (Gaertn.) Voss (salak fruit or snake fruit) is a species of palm tree native to Southwest Java and North Sumatra in Indonesia. It is known as one of the tropical fruits in Malaysia. It is a reddish-brown scaly skin with pleasant pineapple, pear and banana-like aromas. Its strong pleasant aroma, S. zalacca has high potentiality in the perfumery and pharmaceutical industries. The volatile aromas of plants are usually extracted by conventional extraction methods such as steam distillation and solvent extraction methods. These methods are laborious, have incomplete extraction process, require long extraction time, and produced hazardous chemical wastes. A new extraction technique supercritical fluid extraction (SFE) were introduced in this study to overcome these limitations. It is rapidly gaining attention due to its superior benefits over the conventional extraction methods. In this study, the volatile aromas of S. zalacca were extracted by steam distillation, solvents extraction with hexane, diethyl ether and dichloromethane (DCM), and SFE. Carbon dioxide was used for the supercritical fluid. The efficiency and percentage yield of these aromas were compared. The percentage yields by SFE extracts were observed (10 MPa, 30 °C: 0.2577 %; 25 MPa, 50 °C: 0.2375 %; 40 MPa, 70 °C: 0.2721 %) and then the steam distillation (0.1855 %), diethyl ether (0.5692 %), hexane (0.0511 %) and DCM (0.1358 %) were obtained. However, SFE produced a bit lower yield (40 MPa, 70 °C: 0.2721 %) than the diethyl ether solvent extraction (0.5692 %). Over all, SFE was found to be more efficient, environmentally friendly and a produce a satisfactory amount of extract by this SFE required shorter extraction time and a small amount of sample. Oriental Scientific Publishing Company 2019-12-04 Article PeerReviewed application/pdf en http://irep.iium.edu.my/76962/29/OJC_Vol35_No6_p_1669-1677-Salak-2019.pdf application/pdf en http://irep.iium.edu.my/76962/2/OJC%20Copy%20right%20form-2019%20%283%29mysign.pdf application/pdf en http://irep.iium.edu.my/76962/18/email%20evidence.pdf application/pdf en http://irep.iium.edu.my/76962/19/acceptance%20letter.pdf Hilmi, Nur Nadhirah and Mat So'ad, Siti Zaiton and Siddiqui, Mohammad Jamshed Ahmad and Sarker, Md. Zaidul Islam and Rahman, Md. Mokhlesur and Juahir, Hafizan and Raja Hussin, Tengku Mohammad Ariff and Wan Nik, Wan Mohd Norsani and Siddique, Md Nurul Islam (2019) The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss. Oriental Journal of Chemistry, 35 (6). pp. 1669-1677. ISSN 0970 - 020X E-ISSN 2231-5039 http://www.orientjchem.org/
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
English
English
English
topic QD Chemistry
spellingShingle QD Chemistry
Hilmi, Nur Nadhirah
Mat So'ad, Siti Zaiton
Siddiqui, Mohammad Jamshed Ahmad
Sarker, Md. Zaidul Islam
Rahman, Md. Mokhlesur
Juahir, Hafizan
Raja Hussin, Tengku Mohammad Ariff
Wan Nik, Wan Mohd Norsani
Siddique, Md Nurul Islam
The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
description Salacca zalacca (Gaertn.) Voss (salak fruit or snake fruit) is a species of palm tree native to Southwest Java and North Sumatra in Indonesia. It is known as one of the tropical fruits in Malaysia. It is a reddish-brown scaly skin with pleasant pineapple, pear and banana-like aromas. Its strong pleasant aroma, S. zalacca has high potentiality in the perfumery and pharmaceutical industries. The volatile aromas of plants are usually extracted by conventional extraction methods such as steam distillation and solvent extraction methods. These methods are laborious, have incomplete extraction process, require long extraction time, and produced hazardous chemical wastes. A new extraction technique supercritical fluid extraction (SFE) were introduced in this study to overcome these limitations. It is rapidly gaining attention due to its superior benefits over the conventional extraction methods. In this study, the volatile aromas of S. zalacca were extracted by steam distillation, solvents extraction with hexane, diethyl ether and dichloromethane (DCM), and SFE. Carbon dioxide was used for the supercritical fluid. The efficiency and percentage yield of these aromas were compared. The percentage yields by SFE extracts were observed (10 MPa, 30 °C: 0.2577 %; 25 MPa, 50 °C: 0.2375 %; 40 MPa, 70 °C: 0.2721 %) and then the steam distillation (0.1855 %), diethyl ether (0.5692 %), hexane (0.0511 %) and DCM (0.1358 %) were obtained. However, SFE produced a bit lower yield (40 MPa, 70 °C: 0.2721 %) than the diethyl ether solvent extraction (0.5692 %). Over all, SFE was found to be more efficient, environmentally friendly and a produce a satisfactory amount of extract by this SFE required shorter extraction time and a small amount of sample.
format Article
author Hilmi, Nur Nadhirah
Mat So'ad, Siti Zaiton
Siddiqui, Mohammad Jamshed Ahmad
Sarker, Md. Zaidul Islam
Rahman, Md. Mokhlesur
Juahir, Hafizan
Raja Hussin, Tengku Mohammad Ariff
Wan Nik, Wan Mohd Norsani
Siddique, Md Nurul Islam
author_facet Hilmi, Nur Nadhirah
Mat So'ad, Siti Zaiton
Siddiqui, Mohammad Jamshed Ahmad
Sarker, Md. Zaidul Islam
Rahman, Md. Mokhlesur
Juahir, Hafizan
Raja Hussin, Tengku Mohammad Ariff
Wan Nik, Wan Mohd Norsani
Siddique, Md Nurul Islam
author_sort Hilmi, Nur Nadhirah
title The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
title_short The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
title_full The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
title_fullStr The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
title_full_unstemmed The superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from Salacca zalacca (Gaernt..)Voss.
title_sort superioty of supercritical fluid extraction over steam distillation and solvent extraction methods for the extraction of aroma from salacca zalacca (gaernt..)voss.
publisher Oriental Scientific Publishing Company
publishDate 2019
url http://irep.iium.edu.my/76962/
http://irep.iium.edu.my/76962/
http://irep.iium.edu.my/76962/29/OJC_Vol35_No6_p_1669-1677-Salak-2019.pdf
http://irep.iium.edu.my/76962/2/OJC%20Copy%20right%20form-2019%20%283%29mysign.pdf
http://irep.iium.edu.my/76962/18/email%20evidence.pdf
http://irep.iium.edu.my/76962/19/acceptance%20letter.pdf
first_indexed 2023-09-18T21:48:40Z
last_indexed 2023-09-18T21:48:40Z
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