Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach

: Background: Natural deep eutectic solvents (NADESs) can be used for extracting a wide range of biomaterials, such as pectin. This study introduces a new generation of natural solvents for pectin extraction which could replace the conventional solvents in the food industry. Methods: In this stud...

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Main Authors:	Elgharbawy, Amal A.M., Hayyan, Adeeb, Hayyan, Maan, Mirghani, Mohamed Elwathig Saeed, Mohd. Salleh, Hamzah, Rashid, Shahidah Nusailah, Ngoh, Gek Cheng, Liew, Shan Qin, Mohd Nor, Mohd Roslan, Zulkifli, Mohd Zamani, Alias, Yatimah
Format:	Article
Language:	English English
Published:	MDPI 2019
Subjects:	TP Chemical technology TP248.13 Biotechnology
Online Access:	http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/9/73049%20Natural%20Deep%20Eutectic.pdf http://irep.iium.edu.my/73049/15/73049_Natural%20deep%20eutectic%20solvent-assisted%20pectin_SCOPUS.pdf

id	iium-73049
recordtype	eprints
spelling	iium-730492019-08-14T07:32:17Z http://irep.iium.edu.my/73049/ Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach Elgharbawy, Amal A.M. Hayyan, Adeeb Hayyan, Maan Mirghani, Mohamed Elwathig Saeed Mohd. Salleh, Hamzah Rashid, Shahidah Nusailah Ngoh, Gek Cheng Liew, Shan Qin Mohd Nor, Mohd Roslan Zulkifli, Mohd Zamani Alias, Yatimah TP Chemical technology TP248.13 Biotechnology : Background: Natural deep eutectic solvents (NADESs) can be used for extracting a wide range of biomaterials, such as pectin. This study introduces a new generation of natural solvents for pectin extraction which could replace the conventional solvents in the food industry. Methods: In this study, NADESs were used for pectin extraction from pomelo (Citrus grandis (L.) Osbeck) peels using a sonoreactor. Definitive screening design (DSD) was used to screen the influence of time, temperature, solid/liquid ratio, and NADES/water ratio on the pectin yield and degree of esterification (DE). Results: The primary screening revealed that the best choices for the extraction were choline chloride–malonic acid (ChCl-Mal) and choline chloride–glucose–water (ChCl:Glc:W). Both co-solvents yielded 94% pectin and 52% DE after optimization at 80 ◦C, with 60 min of sonication, pH < 3.0, and a NADES-to-water ratio of 1:4.5 (v/v). Morphological screening showed a smooth and compact surface of the pectin from ChCl-Mal where glucose-based pectin had a rough surface and lower DE. Conclusions: NADESs proved to be promising co-solvents for pectin extraction with a high degree of esterification (>55%). MDPI 2019 Article PeerReviewed application/pdf en http://irep.iium.edu.my/73049/9/73049%20Natural%20Deep%20Eutectic.pdf application/pdf en http://irep.iium.edu.my/73049/15/73049_Natural%20deep%20eutectic%20solvent-assisted%20pectin_SCOPUS.pdf Elgharbawy, Amal A.M. and Hayyan, Adeeb and Hayyan, Maan and Mirghani, Mohamed Elwathig Saeed and Mohd. Salleh, Hamzah and Rashid, Shahidah Nusailah and Ngoh, Gek Cheng and Liew, Shan Qin and Mohd Nor, Mohd Roslan and Zulkifli, Mohd Zamani and Alias, Yatimah (2019) Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach. Processes, 7 (7). pp. 1-19. E-ISSN 2227-9717 https://www.mdpi.com/2227-9717/7/7/416/htm 10.3390/pr7070416
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English English
topic	TP Chemical technology TP248.13 Biotechnology
spellingShingle	TP Chemical technology TP248.13 Biotechnology Elgharbawy, Amal A.M. Hayyan, Adeeb Hayyan, Maan Mirghani, Mohamed Elwathig Saeed Mohd. Salleh, Hamzah Rashid, Shahidah Nusailah Ngoh, Gek Cheng Liew, Shan Qin Mohd Nor, Mohd Roslan Zulkifli, Mohd Zamani Alias, Yatimah Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
description	: Background: Natural deep eutectic solvents (NADESs) can be used for extracting a wide range of biomaterials, such as pectin. This study introduces a new generation of natural solvents for pectin extraction which could replace the conventional solvents in the food industry. Methods: In this study, NADESs were used for pectin extraction from pomelo (Citrus grandis (L.) Osbeck) peels using a sonoreactor. Definitive screening design (DSD) was used to screen the influence of time, temperature, solid/liquid ratio, and NADES/water ratio on the pectin yield and degree of esterification (DE). Results: The primary screening revealed that the best choices for the extraction were choline chloride–malonic acid (ChCl-Mal) and choline chloride–glucose–water (ChCl:Glc:W). Both co-solvents yielded 94% pectin and 52% DE after optimization at 80 ◦C, with 60 min of sonication, pH < 3.0, and a NADES-to-water ratio of 1:4.5 (v/v). Morphological screening showed a smooth and compact surface of the pectin from ChCl-Mal where glucose-based pectin had a rough surface and lower DE. Conclusions: NADESs proved to be promising co-solvents for pectin extraction with a high degree of esterification (>55%).
format	Article
author	Elgharbawy, Amal A.M. Hayyan, Adeeb Hayyan, Maan Mirghani, Mohamed Elwathig Saeed Mohd. Salleh, Hamzah Rashid, Shahidah Nusailah Ngoh, Gek Cheng Liew, Shan Qin Mohd Nor, Mohd Roslan Zulkifli, Mohd Zamani Alias, Yatimah
author_facet	Elgharbawy, Amal A.M. Hayyan, Adeeb Hayyan, Maan Mirghani, Mohamed Elwathig Saeed Mohd. Salleh, Hamzah Rashid, Shahidah Nusailah Ngoh, Gek Cheng Liew, Shan Qin Mohd Nor, Mohd Roslan Zulkifli, Mohd Zamani Alias, Yatimah
author_sort	Elgharbawy, Amal A.M.
title	Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
title_short	Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
title_full	Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
title_fullStr	Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
title_full_unstemmed	Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
title_sort	natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach
publisher	MDPI
publishDate	2019
url	http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/ http://irep.iium.edu.my/73049/9/73049%20Natural%20Deep%20Eutectic.pdf http://irep.iium.edu.my/73049/15/73049_Natural%20deep%20eutectic%20solvent-assisted%20pectin_SCOPUS.pdf
first_indexed	2023-09-18T21:43:34Z
last_indexed	2023-09-18T21:43:34Z
_version_	1777413300820115456

Natural deep eutectic solvent-assisted pectin extraction from pomelo peel using sonoreactor: experimental optimization approach

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