Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper
Emerging evidence has revealed the functional characteristics of black pepper extracts for both nutritional and medicinal purposes. The medicinal properties of this important commodity crop are due to the presence of active piperine which it a viable drug potential in ethnomedicine for the treatment...
Main Authors: | , , , , |
---|---|
Format: | Article |
Language: | English English |
Published: |
Elsevier B.V
2018
|
Subjects: | |
Online Access: | http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/1/67179_Chemical%20fingerprinting%20of%20biologically%20active.pdf http://irep.iium.edu.my/67179/7/67179_Chemical%20fingerprinting%20of%20biologically%20active%20compounds-scopus.pdf |
id |
iium-67179 |
---|---|
recordtype |
eprints |
spelling |
iium-671792019-01-08T08:25:15Z http://irep.iium.edu.my/67179/ Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper Olalere, Olusegun Abayomi Abdurahman, Nour Hamid Mohd Yunus, Rosli Alara, Oluwaseun Ruth Kabbashi, Nassereldeen Ahmed TP155 Chemical engineering Emerging evidence has revealed the functional characteristics of black pepper extracts for both nutritional and medicinal purposes. The medicinal properties of this important commodity crop are due to the presence of active piperine which it a viable drug potential in ethnomedicine for the treatment of many degenerative free-radical related diseases. In this study, the mi-crowave-enhanced technique was employed in the extraction of alkaloid oleoresins at optimum condition. The metabolomics-based approach was employed to determine the alkaloid profiles using LC-MS-Quadrupled time of flight mass spectrometer. At optimum microwave condition, a total of 21 bioactive alkaloids were identified with piperine being the most abundant with a mass to charge ratio of 286.1442m/z. The result from the SEM-monograph and BET-surface characterization showed a remarkable transformation in the micro-cellular matrix as a result of the applied microwave electromagnetic heating Elsevier B.V 2018-12 Article PeerReviewed application/pdf en http://irep.iium.edu.my/67179/1/67179_Chemical%20fingerprinting%20of%20biologically%20active.pdf application/pdf en http://irep.iium.edu.my/67179/7/67179_Chemical%20fingerprinting%20of%20biologically%20active%20compounds-scopus.pdf Olalere, Olusegun Abayomi and Abdurahman, Nour Hamid and Mohd Yunus, Rosli and Alara, Oluwaseun Ruth and Kabbashi, Nassereldeen Ahmed (2018) Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper. Chemical Data Collections, 17-18. pp. 339-344. ISSN 2405-8300 https://www.sciencedirect.com/science/article/pii/S2405830018300880 10.1016/j.cdc.2018.10.007 2405-8300 |
repository_type |
Digital Repository |
institution_category |
Local University |
institution |
International Islamic University Malaysia |
building |
IIUM Repository |
collection |
Online Access |
language |
English English |
topic |
TP155 Chemical engineering |
spellingShingle |
TP155 Chemical engineering Olalere, Olusegun Abayomi Abdurahman, Nour Hamid Mohd Yunus, Rosli Alara, Oluwaseun Ruth Kabbashi, Nassereldeen Ahmed Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
description |
Emerging evidence has revealed the functional characteristics of black pepper extracts for both nutritional and medicinal purposes. The medicinal properties of this important commodity crop are due to the presence of active piperine which it a viable drug potential in ethnomedicine for the treatment of many degenerative free-radical related diseases. In this study, the mi-crowave-enhanced technique was employed in the extraction of alkaloid oleoresins at optimum condition. The metabolomics-based approach was employed to determine the alkaloid profiles using LC-MS-Quadrupled time of flight mass spectrometer. At optimum microwave condition, a total of 21 bioactive alkaloids were identified with piperine being the most abundant with a mass to charge ratio of 286.1442m/z. The result from the SEM-monograph and BET-surface characterization showed a remarkable transformation in the micro-cellular matrix as a result of the applied microwave electromagnetic heating |
format |
Article |
author |
Olalere, Olusegun Abayomi Abdurahman, Nour Hamid Mohd Yunus, Rosli Alara, Oluwaseun Ruth Kabbashi, Nassereldeen Ahmed |
author_facet |
Olalere, Olusegun Abayomi Abdurahman, Nour Hamid Mohd Yunus, Rosli Alara, Oluwaseun Ruth Kabbashi, Nassereldeen Ahmed |
author_sort |
Olalere, Olusegun Abayomi |
title |
Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
title_short |
Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
title_full |
Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
title_fullStr |
Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
title_full_unstemmed |
Chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
title_sort |
chemical fingerprinting of biologically active compounds morphological transformation during microwave reflux extraction of black pepper |
publisher |
Elsevier B.V |
publishDate |
2018 |
url |
http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/ http://irep.iium.edu.my/67179/1/67179_Chemical%20fingerprinting%20of%20biologically%20active.pdf http://irep.iium.edu.my/67179/7/67179_Chemical%20fingerprinting%20of%20biologically%20active%20compounds-scopus.pdf |
first_indexed |
2023-09-18T21:35:23Z |
last_indexed |
2023-09-18T21:35:23Z |
_version_ |
1777412785432428544 |