Synthesis and characterization of silica ceramic membranes via sol-dip coating

The application of inorganic membrane as one of the methods for gas separation process has proven to show the greatest potential when compared to other methods. Ceramic membranes are considered as one of the many high potential inorganic membranes for this purpose. Current development of ceramic mem...

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Main Authors: Kahlib, Nor Amyra Zulianey, Mohd Daud, Farah Diana, Mel, Maizirwan, Ahmad Azhar, Ahmad Zahirani, Hassan, Noor Azlina
Format: Article
Language:English
Published: Penerbit Akademia Baru 2017
Subjects:
Online Access:http://irep.iium.edu.my/59555/
http://irep.iium.edu.my/59555/1/59555_Synthesis%20and%20characterization%20of%20silica.pdf
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recordtype eprints
spelling iium-595552018-03-21T03:35:43Z http://irep.iium.edu.my/59555/ Synthesis and characterization of silica ceramic membranes via sol-dip coating Kahlib, Nor Amyra Zulianey Mohd Daud, Farah Diana Mel, Maizirwan Ahmad Azhar, Ahmad Zahirani Hassan, Noor Azlina TA Engineering (General). Civil engineering (General) TA401 Materials of engineering and construction The application of inorganic membrane as one of the methods for gas separation process has proven to show the greatest potential when compared to other methods. Ceramic membranes are considered as one of the many high potential inorganic membranes for this purpose. Current development of ceramic membrane focuses on the reduction of pore size for ceramic membrane up to nanometer scale without pinholes or cracking. Thus, in recent work, the silica ceramic membranes via sol dip-coating have been synthesized by using tetraethylorthosilicate (TEOS), distilled water and ethyl alcohol as sol. The influences of number of dipping have been examined. X-ray diffraction (XRD) results of the fabricated silica membrane show the presence of silica element and that each membrane possesses a periodic structure with each number of dipping. The IR adsorption from Fourier transform infrared spectrometry (FTIR) indicates the presence of functional group O-Si-O and Si-CH3. The intensity of these functional groups increases as the dipping time increase. Field Emission Scanning Electron Microscope (FESEM) results show that the number of visible pores on the surface of the ceramic support diminished after modification of ceramic membrane, with the number of silica particles increasing linearly with number of dipping. Thus, the synthesized silica ceramic membrane with good structure and chemical properties has shown great potential for biogas separation application. Penerbit Akademia Baru 2017-12 Article PeerReviewed application/pdf en http://irep.iium.edu.my/59555/1/59555_Synthesis%20and%20characterization%20of%20silica.pdf Kahlib, Nor Amyra Zulianey and Mohd Daud, Farah Diana and Mel, Maizirwan and Ahmad Azhar, Ahmad Zahirani and Hassan, Noor Azlina (2017) Synthesis and characterization of silica ceramic membranes via sol-dip coating. Journal of Advanced Research in Materials Science, 39 (1). pp. 1-7. ISSN 2289-7992
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
topic TA Engineering (General). Civil engineering (General)
TA401 Materials of engineering and construction
spellingShingle TA Engineering (General). Civil engineering (General)
TA401 Materials of engineering and construction
Kahlib, Nor Amyra Zulianey
Mohd Daud, Farah Diana
Mel, Maizirwan
Ahmad Azhar, Ahmad Zahirani
Hassan, Noor Azlina
Synthesis and characterization of silica ceramic membranes via sol-dip coating
description The application of inorganic membrane as one of the methods for gas separation process has proven to show the greatest potential when compared to other methods. Ceramic membranes are considered as one of the many high potential inorganic membranes for this purpose. Current development of ceramic membrane focuses on the reduction of pore size for ceramic membrane up to nanometer scale without pinholes or cracking. Thus, in recent work, the silica ceramic membranes via sol dip-coating have been synthesized by using tetraethylorthosilicate (TEOS), distilled water and ethyl alcohol as sol. The influences of number of dipping have been examined. X-ray diffraction (XRD) results of the fabricated silica membrane show the presence of silica element and that each membrane possesses a periodic structure with each number of dipping. The IR adsorption from Fourier transform infrared spectrometry (FTIR) indicates the presence of functional group O-Si-O and Si-CH3. The intensity of these functional groups increases as the dipping time increase. Field Emission Scanning Electron Microscope (FESEM) results show that the number of visible pores on the surface of the ceramic support diminished after modification of ceramic membrane, with the number of silica particles increasing linearly with number of dipping. Thus, the synthesized silica ceramic membrane with good structure and chemical properties has shown great potential for biogas separation application.
format Article
author Kahlib, Nor Amyra Zulianey
Mohd Daud, Farah Diana
Mel, Maizirwan
Ahmad Azhar, Ahmad Zahirani
Hassan, Noor Azlina
author_facet Kahlib, Nor Amyra Zulianey
Mohd Daud, Farah Diana
Mel, Maizirwan
Ahmad Azhar, Ahmad Zahirani
Hassan, Noor Azlina
author_sort Kahlib, Nor Amyra Zulianey
title Synthesis and characterization of silica ceramic membranes via sol-dip coating
title_short Synthesis and characterization of silica ceramic membranes via sol-dip coating
title_full Synthesis and characterization of silica ceramic membranes via sol-dip coating
title_fullStr Synthesis and characterization of silica ceramic membranes via sol-dip coating
title_full_unstemmed Synthesis and characterization of silica ceramic membranes via sol-dip coating
title_sort synthesis and characterization of silica ceramic membranes via sol-dip coating
publisher Penerbit Akademia Baru
publishDate 2017
url http://irep.iium.edu.my/59555/
http://irep.iium.edu.my/59555/1/59555_Synthesis%20and%20characterization%20of%20silica.pdf
first_indexed 2023-09-18T21:24:23Z
last_indexed 2023-09-18T21:24:23Z
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