Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.

Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by...

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Main Authors: K. Saurabh, Chaturbhuj, Dungani, Rudi, A.F., Owolabi, N.S., Atiqah, Ashaari, Zaidon, N. A., Sri Aprilia, Sarker, Md. Zaidul Islam, H. P. S., Abdul Khalil
Format: Article
Language:English
English
Published: NC State University 2016
Subjects:
Online Access:http://irep.iium.edu.my/53855/
http://irep.iium.edu.my/53855/
http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf
http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf
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spelling iium-538552017-04-13T07:03:00Z http://irep.iium.edu.my/53855/ Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. K. Saurabh, Chaturbhuj Dungani, Rudi A.F., Owolabi N.S., Atiqah Ashaari, Zaidon N. A., Sri Aprilia Sarker, Md. Zaidul Islam H. P. S., Abdul Khalil R Medicine (General) Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by sulphuric acid hydrolysis having different time duration of hydrolysis. Apart from the progressive reduction in peaks characteristic of hemicellulose and lignin dissolution, FTIR spectroscopy analysis showed that the hydrolysis did not affect the chemical structure of CNW was revealed by TEM. XRD analysis revealed that the natural structural of cellulose I polymorph was mantained irrespective of the hydrolysis time. High thermal stability and aspect ratio of the extracted CNW demostrated its suitability as a reinforcement material in nanocomposites. NC State University 2016 Article PeerReviewed application/pdf en http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf application/pdf en http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf K. Saurabh, Chaturbhuj and Dungani, Rudi and A.F., Owolabi and N.S., Atiqah and Ashaari, Zaidon and N. A., Sri Aprilia and Sarker, Md. Zaidul Islam and H. P. S., Abdul Khalil (2016) Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics. BioResources, 11 (3). pp. 6742-6755. ISSN 1930-2126 http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_3_6742_Saurabh_Hydrolysis_Cellulose_Nanowhiskers
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
English
topic R Medicine (General)
spellingShingle R Medicine (General)
K. Saurabh, Chaturbhuj
Dungani, Rudi
A.F., Owolabi
N.S., Atiqah
Ashaari, Zaidon
N. A., Sri Aprilia
Sarker, Md. Zaidul Islam
H. P. S., Abdul Khalil
Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
description Oil palm fronds biomass was used as a source for isolation of cellulose nanowhiskers (CNW), and its subsequent characterization was done. Non-cellulosic components such a lignin, hemicellulose, and pectin were removed from the biomass by chemimechanical alkaline hydrogen peroxide method followed by sulphuric acid hydrolysis having different time duration of hydrolysis. Apart from the progressive reduction in peaks characteristic of hemicellulose and lignin dissolution, FTIR spectroscopy analysis showed that the hydrolysis did not affect the chemical structure of CNW was revealed by TEM. XRD analysis revealed that the natural structural of cellulose I polymorph was mantained irrespective of the hydrolysis time. High thermal stability and aspect ratio of the extracted CNW demostrated its suitability as a reinforcement material in nanocomposites.
format Article
author K. Saurabh, Chaturbhuj
Dungani, Rudi
A.F., Owolabi
N.S., Atiqah
Ashaari, Zaidon
N. A., Sri Aprilia
Sarker, Md. Zaidul Islam
H. P. S., Abdul Khalil
author_facet K. Saurabh, Chaturbhuj
Dungani, Rudi
A.F., Owolabi
N.S., Atiqah
Ashaari, Zaidon
N. A., Sri Aprilia
Sarker, Md. Zaidul Islam
H. P. S., Abdul Khalil
author_sort K. Saurabh, Chaturbhuj
title Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
title_short Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
title_full Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
title_fullStr Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
title_full_unstemmed Effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (Elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
title_sort effect of hydrolysis treatment on cellulose nanowhiskers from oil palm (elaeis guineesis) fronds: morphology, chemical, crystallinity, and thermal characteristics.
publisher NC State University
publishDate 2016
url http://irep.iium.edu.my/53855/
http://irep.iium.edu.my/53855/
http://irep.iium.edu.my/53855/1/BioRes_11_3_6742_Saurabh_DOSZASK_Effect_Hydroly_Treat_CNW_Oil_Palm_Fronds_9745.pdf
http://irep.iium.edu.my/53855/7/53855_Effect%20of%20hydrolysis%20treatment%20on%20cellulose_wos.pdf
first_indexed 2023-09-18T21:16:11Z
last_indexed 2023-09-18T21:16:11Z
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