Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders

Dense manganese-doped biphasic calcium phosphate (Mn-BCP) ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were sintered in ambient atmosphere with temperatures ranging from 800�C to 1400�C. Manganese (Mn) level was varied in the range of 0.6, 1...

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Main Authors:	Sopyan, Iis, Nawawi, Natasha Ahmad, Shah, Qasim Hussain, Ramesh, Singh, Tan, Chou Yong, Abd Shukor, Mohd Hamdi
Format:	Article
Language:	English
Published:	Taylor & Francis 2011
Subjects:	TS200 Metal manufactures. Metalworking
Online Access:	http://irep.iium.edu.my/4284/ http://irep.iium.edu.my/4284/ http://irep.iium.edu.my/4284/1/MMP_paper.pdf

id	iium-4284
recordtype	eprints
spelling	iium-42842013-07-02T04:57:54Z http://irep.iium.edu.my/4284/ Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders Sopyan, Iis Nawawi, Natasha Ahmad Shah, Qasim Hussain Ramesh, Singh Tan, Chou Yong Abd Shukor, Mohd Hamdi TS200 Metal manufactures. Metalworking Dense manganese-doped biphasic calcium phosphate (Mn-BCP) ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were sintered in ambient atmosphere with temperatures ranging from 800�C to 1400�C. Manganese (Mn) level was varied in the range of 0.6, 1.9, 4.3, and 11.9mol%, and its effect on physical and mechanical properties of the dense samples were investigated. All dense samples have been proved to show HA and �-TCP phases only. Mn doping has shifted the onset of the sintering temperature of the BCP, leading to the improved densification of BCP ceramics. The relative density also increased with sintering temperature. Considerable grain growth has been observed for Mn-doped BCP samples when compared to the undoped BCP. Furthermore, 11.9mol% Mn-doped BCP dense samples showed the maximum hardness of 6.66GPa compared to 2.89 GPa for the undoped BCP. The incorporation of Mn was also found to be beneficial in enhancing the fracture toughness of BCP throughout the temperature range employed. This study has shown that Mn doping was effective in improving the sintering properties of BCP without affecting the phase stability. Taylor & Francis 2011-06-27 Article PeerReviewed application/pdf en http://irep.iium.edu.my/4284/1/MMP_paper.pdf Sopyan, Iis and Nawawi, Natasha Ahmad and Shah, Qasim Hussain and Ramesh, Singh and Tan, Chou Yong and Abd Shukor, Mohd Hamdi (2011) Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders. Materials and Manufacturing Processes, 26. pp. 908-914. ISSN 1532-2475 ; 1042-6914 http://www.tandf.co.uk/journals/lmmp
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	TS200 Metal manufactures. Metalworking
spellingShingle	TS200 Metal manufactures. Metalworking Sopyan, Iis Nawawi, Natasha Ahmad Shah, Qasim Hussain Ramesh, Singh Tan, Chou Yong Abd Shukor, Mohd Hamdi Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
description	Dense manganese-doped biphasic calcium phosphate (Mn-BCP) ceramics were fabricated via uniaxial pressing using the sol-gel derived powders. The compacted discs were sintered in ambient atmosphere with temperatures ranging from 800�C to 1400�C. Manganese (Mn) level was varied in the range of 0.6, 1.9, 4.3, and 11.9mol%, and its effect on physical and mechanical properties of the dense samples were investigated. All dense samples have been proved to show HA and �-TCP phases only. Mn doping has shifted the onset of the sintering temperature of the BCP, leading to the improved densification of BCP ceramics. The relative density also increased with sintering temperature. Considerable grain growth has been observed for Mn-doped BCP samples when compared to the undoped BCP. Furthermore, 11.9mol% Mn-doped BCP dense samples showed the maximum hardness of 6.66GPa compared to 2.89 GPa for the undoped BCP. The incorporation of Mn was also found to be beneficial in enhancing the fracture toughness of BCP throughout the temperature range employed. This study has shown that Mn doping was effective in improving the sintering properties of BCP without affecting the phase stability.
format	Article
author	Sopyan, Iis Nawawi, Natasha Ahmad Shah, Qasim Hussain Ramesh, Singh Tan, Chou Yong Abd Shukor, Mohd Hamdi
author_facet	Sopyan, Iis Nawawi, Natasha Ahmad Shah, Qasim Hussain Ramesh, Singh Tan, Chou Yong Abd Shukor, Mohd Hamdi
author_sort	Sopyan, Iis
title	Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
title_short	Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
title_full	Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
title_fullStr	Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
title_full_unstemmed	Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
title_sort	sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders
publisher	Taylor & Francis
publishDate	2011
url	http://irep.iium.edu.my/4284/ http://irep.iium.edu.my/4284/ http://irep.iium.edu.my/4284/1/MMP_paper.pdf
first_indexed	2023-09-18T20:12:27Z
last_indexed	2023-09-18T20:12:27Z
_version_	1777407568578084864

Sintering and properties of dense manganese-doped calcium phosphate bioceramics prepared using sol-gel derived nanopowders

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