Optimisation of the supercritical extraction of toxic elements in fish oil
This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil. The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central composite design (CCD) of response surface meth...
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iium-389532018-06-19T06:31:57Z http://irep.iium.edu.my/38953/ Optimisation of the supercritical extraction of toxic elements in fish oil Hajeb, Parvaneh Jinap, S. Shakibazadeh, Sh. Afsah-Hejri, L. Mohebbi, G.H. Sarker, Md. Zaidul Islam Q Science (General) T Technology (General) This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil. The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central composite design (CCD) of response surface methodology (RSM). High coefficients of determination (R2 ) (0.897–0.988) for the predicted response surface models confirmed a satisfactory adjustment of the polynomial regression models with the operation conditions. The results showed that the linear and quadratic terms of pressure and temperature were the most significant (p < 0.05) variables affecting the overall responses. The optimum conditions for the simultaneous elimination of toxic elements comprised a pressure of 61 MPa, a temperature of 39.8ºC, a CO2 flow rate of 3.7 ml min−1 and an extraction time of 4 h. These optimised SFE conditions were able to produce fish oil with the contents of lead, cadmium, arsenic and mercury reduced by up to 98.3%, 96.1%, 94.9% and 93.7%, respectively. The fish oil extracted under the optimised SFE operating conditions was of good quality in terms of its fatty acid constituents. Taylor and Francis 2014-07-03 Article PeerReviewed application/pdf en http://irep.iium.edu.my/38953/1/Food_Additives_Contaminants.pdf Hajeb, Parvaneh and Jinap, S. and Shakibazadeh, Sh. and Afsah-Hejri, L. and Mohebbi, G.H. and Sarker, Md. Zaidul Islam (2014) Optimisation of the supercritical extraction of toxic elements in fish oil. Food Additives & Contaminants: Part A, 31 (10). pp. 1712-1722. ISSN 1944-0049 http://www.tandfonline.com/toc/tfac20/current#.VFH8G1HzTFY 10.1080/19440049.2014.942707 |
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Q Science (General) T Technology (General) Hajeb, Parvaneh Jinap, S. Shakibazadeh, Sh. Afsah-Hejri, L. Mohebbi, G.H. Sarker, Md. Zaidul Islam Optimisation of the supercritical extraction of toxic elements in fish oil |
description |
This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil.
The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central
composite design (CCD) of response surface methodology (RSM). High coefficients of determination (R2
) (0.897–0.988) for
the predicted response surface models confirmed a satisfactory adjustment of the polynomial regression models with the
operation conditions. The results showed that the linear and quadratic terms of pressure and temperature were the most
significant (p < 0.05) variables affecting the overall responses. The optimum conditions for the simultaneous elimination of
toxic elements comprised a pressure of 61 MPa, a temperature of 39.8ºC, a CO2 flow rate of 3.7 ml min−1 and an extraction
time of 4 h. These optimised SFE conditions were able to produce fish oil with the contents of lead, cadmium, arsenic and
mercury reduced by up to 98.3%, 96.1%, 94.9% and 93.7%, respectively. The fish oil extracted under the optimised SFE
operating conditions was of good quality in terms of its fatty acid constituents. |
format |
Article |
author |
Hajeb, Parvaneh Jinap, S. Shakibazadeh, Sh. Afsah-Hejri, L. Mohebbi, G.H. Sarker, Md. Zaidul Islam |
author_facet |
Hajeb, Parvaneh Jinap, S. Shakibazadeh, Sh. Afsah-Hejri, L. Mohebbi, G.H. Sarker, Md. Zaidul Islam |
author_sort |
Hajeb, Parvaneh |
title |
Optimisation of the supercritical extraction of toxic
elements in fish oil |
title_short |
Optimisation of the supercritical extraction of toxic
elements in fish oil |
title_full |
Optimisation of the supercritical extraction of toxic
elements in fish oil |
title_fullStr |
Optimisation of the supercritical extraction of toxic
elements in fish oil |
title_full_unstemmed |
Optimisation of the supercritical extraction of toxic
elements in fish oil |
title_sort |
optimisation of the supercritical extraction of toxic
elements in fish oil |
publisher |
Taylor and Francis |
publishDate |
2014 |
url |
http://irep.iium.edu.my/38953/ http://irep.iium.edu.my/38953/ http://irep.iium.edu.my/38953/ http://irep.iium.edu.my/38953/1/Food_Additives_Contaminants.pdf |
first_indexed |
2023-09-18T20:55:58Z |
last_indexed |
2023-09-18T20:55:58Z |
_version_ |
1777410305896218624 |