Optimisation of the supercritical extraction of toxic elements in fish oil

This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil. The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central composite design (CCD) of response surface meth...

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Main Authors: Hajeb, Parvaneh, Jinap, S., Shakibazadeh, Sh., Afsah-Hejri, L., Mohebbi, G.H., Sarker, Md. Zaidul Islam
Format: Article
Language:English
Published: Taylor and Francis 2014
Subjects:
Online Access:http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/1/Food_Additives_Contaminants.pdf
id iium-38953
recordtype eprints
spelling iium-389532018-06-19T06:31:57Z http://irep.iium.edu.my/38953/ Optimisation of the supercritical extraction of toxic elements in fish oil Hajeb, Parvaneh Jinap, S. Shakibazadeh, Sh. Afsah-Hejri, L. Mohebbi, G.H. Sarker, Md. Zaidul Islam Q Science (General) T Technology (General) This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil. The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central composite design (CCD) of response surface methodology (RSM). High coefficients of determination (R2 ) (0.897–0.988) for the predicted response surface models confirmed a satisfactory adjustment of the polynomial regression models with the operation conditions. The results showed that the linear and quadratic terms of pressure and temperature were the most significant (p < 0.05) variables affecting the overall responses. The optimum conditions for the simultaneous elimination of toxic elements comprised a pressure of 61 MPa, a temperature of 39.8ºC, a CO2 flow rate of 3.7 ml min−1 and an extraction time of 4 h. These optimised SFE conditions were able to produce fish oil with the contents of lead, cadmium, arsenic and mercury reduced by up to 98.3%, 96.1%, 94.9% and 93.7%, respectively. The fish oil extracted under the optimised SFE operating conditions was of good quality in terms of its fatty acid constituents. Taylor and Francis 2014-07-03 Article PeerReviewed application/pdf en http://irep.iium.edu.my/38953/1/Food_Additives_Contaminants.pdf Hajeb, Parvaneh and Jinap, S. and Shakibazadeh, Sh. and Afsah-Hejri, L. and Mohebbi, G.H. and Sarker, Md. Zaidul Islam (2014) Optimisation of the supercritical extraction of toxic elements in fish oil. Food Additives & Contaminants: Part A, 31 (10). pp. 1712-1722. ISSN 1944-0049 http://www.tandfonline.com/toc/tfac20/current#.VFH8G1HzTFY 10.1080/19440049.2014.942707
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
topic Q Science (General)
T Technology (General)
spellingShingle Q Science (General)
T Technology (General)
Hajeb, Parvaneh
Jinap, S.
Shakibazadeh, Sh.
Afsah-Hejri, L.
Mohebbi, G.H.
Sarker, Md. Zaidul Islam
Optimisation of the supercritical extraction of toxic elements in fish oil
description This study aims to optimise the operating conditions for the supercritical fluid extraction (SFE) of toxic elements from fish oil. The SFE operating parameters of pressure, temperature, CO2 flow rate and extraction time were optimised using a central composite design (CCD) of response surface methodology (RSM). High coefficients of determination (R2 ) (0.897–0.988) for the predicted response surface models confirmed a satisfactory adjustment of the polynomial regression models with the operation conditions. The results showed that the linear and quadratic terms of pressure and temperature were the most significant (p < 0.05) variables affecting the overall responses. The optimum conditions for the simultaneous elimination of toxic elements comprised a pressure of 61 MPa, a temperature of 39.8ºC, a CO2 flow rate of 3.7 ml min−1 and an extraction time of 4 h. These optimised SFE conditions were able to produce fish oil with the contents of lead, cadmium, arsenic and mercury reduced by up to 98.3%, 96.1%, 94.9% and 93.7%, respectively. The fish oil extracted under the optimised SFE operating conditions was of good quality in terms of its fatty acid constituents.
format Article
author Hajeb, Parvaneh
Jinap, S.
Shakibazadeh, Sh.
Afsah-Hejri, L.
Mohebbi, G.H.
Sarker, Md. Zaidul Islam
author_facet Hajeb, Parvaneh
Jinap, S.
Shakibazadeh, Sh.
Afsah-Hejri, L.
Mohebbi, G.H.
Sarker, Md. Zaidul Islam
author_sort Hajeb, Parvaneh
title Optimisation of the supercritical extraction of toxic elements in fish oil
title_short Optimisation of the supercritical extraction of toxic elements in fish oil
title_full Optimisation of the supercritical extraction of toxic elements in fish oil
title_fullStr Optimisation of the supercritical extraction of toxic elements in fish oil
title_full_unstemmed Optimisation of the supercritical extraction of toxic elements in fish oil
title_sort optimisation of the supercritical extraction of toxic elements in fish oil
publisher Taylor and Francis
publishDate 2014
url http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/
http://irep.iium.edu.my/38953/1/Food_Additives_Contaminants.pdf
first_indexed 2023-09-18T20:55:58Z
last_indexed 2023-09-18T20:55:58Z
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