Sintering of hydroxyapatite ceramic produced by wet chemical method
In the present work, densification of synthesised hydroxyapatite (HA) bioceramic prepared via chemical precipitation method was investigated. HA samples was prepared by compaction at 200 MPa and sintered at temperatures ranging from 800°C to 1400°C. The results revealed that the HA phase was stable...
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Trans Tech Publications, Switzerland
2011
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iium-214232012-02-24T03:14:42Z http://irep.iium.edu.my/21423/ Sintering of hydroxyapatite ceramic produced by wet chemical method Singh, Ramesh Ranna, Tolouei Tan, Chou Yong K. L., Aw W., H. Yeo Iis, Sopyan Teng, Wan Dung TS Manufactures In the present work, densification of synthesised hydroxyapatite (HA) bioceramic prepared via chemical precipitation method was investigated. HA samples was prepared by compaction at 200 MPa and sintered at temperatures ranging from 800°C to 1400°C. The results revealed that the HA phase was stable for up to sintering temperature of 1250°C. However, decomposition of HA was observed in samples sintered at 1300°C with the formation of tetra-calcium phosphate (TTCP) and CaO. Samples sintered above 1400°C were found to melt into glassy phases. The bulk density increases with increasing temperature and attained a maximum value of 3.14 gcm-3 at 1150°C whereas maximum hardness value of 6.64 GPa was measured in HA sintered at 1050°C. These results are discussed in terms of the role of grain size. © (2011) Trans Tech Publications, Switzerland. Trans Tech Publications, Switzerland 2011-06-30 Article PeerReviewed application/pdf en http://irep.iium.edu.my/21423/1/AMR.264-265.1856_9.pdf Singh, Ramesh and Ranna, Tolouei and Tan, Chou Yong and K. L., Aw and W., H. Yeo and Iis, Sopyan and Teng, Wan Dung (2011) Sintering of hydroxyapatite ceramic produced by wet chemical method. Advanced Materials Research, 264/65. pp. 1856-1861. ISSN 1022-6680 http://www.scientific.net/AMR.264-265.1856 10.4028/www.scientific.net/AMR.264-265.1856 |
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TS Manufactures Singh, Ramesh Ranna, Tolouei Tan, Chou Yong K. L., Aw W., H. Yeo Iis, Sopyan Teng, Wan Dung Sintering of hydroxyapatite ceramic produced by wet chemical method |
description |
In the present work, densification of synthesised hydroxyapatite (HA) bioceramic prepared via chemical precipitation method was investigated. HA samples was prepared by compaction at 200 MPa and sintered at temperatures ranging from 800°C to 1400°C. The results revealed that the HA phase was stable for up to sintering temperature of 1250°C. However, decomposition of HA was observed in samples sintered at 1300°C with the formation of tetra-calcium phosphate (TTCP) and CaO. Samples sintered above 1400°C were found to melt into glassy phases. The bulk density increases with increasing temperature and attained a maximum value of 3.14 gcm-3 at 1150°C whereas maximum hardness value of 6.64 GPa was measured in HA sintered at 1050°C. These results are discussed in terms of the role of grain size. © (2011) Trans Tech Publications, Switzerland. |
format |
Article |
author |
Singh, Ramesh Ranna, Tolouei Tan, Chou Yong K. L., Aw W., H. Yeo Iis, Sopyan Teng, Wan Dung |
author_facet |
Singh, Ramesh Ranna, Tolouei Tan, Chou Yong K. L., Aw W., H. Yeo Iis, Sopyan Teng, Wan Dung |
author_sort |
Singh, Ramesh |
title |
Sintering of hydroxyapatite ceramic produced by wet chemical method |
title_short |
Sintering of hydroxyapatite ceramic produced by wet chemical method |
title_full |
Sintering of hydroxyapatite ceramic produced by wet chemical method |
title_fullStr |
Sintering of hydroxyapatite ceramic produced by wet chemical method |
title_full_unstemmed |
Sintering of hydroxyapatite ceramic produced by wet chemical method |
title_sort |
sintering of hydroxyapatite ceramic produced by wet chemical method |
publisher |
Trans Tech Publications, Switzerland |
publishDate |
2011 |
url |
http://irep.iium.edu.my/21423/ http://irep.iium.edu.my/21423/ http://irep.iium.edu.my/21423/ http://irep.iium.edu.my/21423/1/AMR.264-265.1856_9.pdf |
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2023-09-18T20:32:32Z |
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2023-09-18T20:32:32Z |
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