Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis

MnxZn1-xFe2O4 nanoparticles with x = 0, 0.2, 0.4, 0.5, 0.6 and 1.0 were synthesized by polymer matrix templated synthesis. Ion exchange resins in a form of spherical beads that contained nanopores were used to precipitate the nanoparticles. The synthesized nanoparticles were characterized using seve...

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Main Authors: Mohd Noor, Siti Salwa, Yaacob, Iskandar Idris
Format: Article
Language:English
Published: Trans Tech Publications, Switzerland 2010
Subjects:
Online Access:http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/1/Preparation_of_Manganese_Zinc_Ferrite_Nanoparticles.pdf
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spelling iium-164122012-02-01T01:05:42Z http://irep.iium.edu.my/16412/ Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis Mohd Noor, Siti Salwa Yaacob, Iskandar Idris TJ Mechanical engineering and machinery MnxZn1-xFe2O4 nanoparticles with x = 0, 0.2, 0.4, 0.5, 0.6 and 1.0 were synthesized by polymer matrix templated synthesis. Ion exchange resins in a form of spherical beads that contained nanopores were used to precipitate the nanoparticles. The synthesized nanoparticles were characterized using several characterization techniques including X-ray diffractometry, transmission electron microscopy and alternating gradient magnetometry. XRD patterns showed that only manganese zinc ferrite nanoparticles were formed. Calculation of crystallite size from x-ray peak broadening showed that the crystallite sizes were within the range 5-11 nm. The crystallite size increased with increasing Mn concentration. TEM images showed that the particles were almost spherical with diameters ranging from 8-19 nm. Magnetization curves passed through the origin and showed no hysteresis indicated that the particles are superparamagnetic. The magnetization value at 10kOe applied magnetic field increased with increasing particle size which was mainly due to the effect of manganese content of the nanoparticles. © (2010) Trans Tech Publications. Trans Tech Publications, Switzerland 2010 Article NonPeerReviewed application/pdf en http://irep.iium.edu.my/16412/1/Preparation_of_Manganese_Zinc_Ferrite_Nanoparticles.pdf Mohd Noor, Siti Salwa and Yaacob, Iskandar Idris (2010) Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis. Advanced Materials Research, 97-101. pp. 2171-2174. ISSN 1022-6680 (Unpublished) http://www.scientific.net/AMR.97-101.2171 10.4028/www.scientific.net/AMR.97-101.2171
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
topic TJ Mechanical engineering and machinery
spellingShingle TJ Mechanical engineering and machinery
Mohd Noor, Siti Salwa
Yaacob, Iskandar Idris
Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
description MnxZn1-xFe2O4 nanoparticles with x = 0, 0.2, 0.4, 0.5, 0.6 and 1.0 were synthesized by polymer matrix templated synthesis. Ion exchange resins in a form of spherical beads that contained nanopores were used to precipitate the nanoparticles. The synthesized nanoparticles were characterized using several characterization techniques including X-ray diffractometry, transmission electron microscopy and alternating gradient magnetometry. XRD patterns showed that only manganese zinc ferrite nanoparticles were formed. Calculation of crystallite size from x-ray peak broadening showed that the crystallite sizes were within the range 5-11 nm. The crystallite size increased with increasing Mn concentration. TEM images showed that the particles were almost spherical with diameters ranging from 8-19 nm. Magnetization curves passed through the origin and showed no hysteresis indicated that the particles are superparamagnetic. The magnetization value at 10kOe applied magnetic field increased with increasing particle size which was mainly due to the effect of manganese content of the nanoparticles. © (2010) Trans Tech Publications.
format Article
author Mohd Noor, Siti Salwa
Yaacob, Iskandar Idris
author_facet Mohd Noor, Siti Salwa
Yaacob, Iskandar Idris
author_sort Mohd Noor, Siti Salwa
title Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
title_short Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
title_full Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
title_fullStr Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
title_full_unstemmed Preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
title_sort preparation of manganese zinc ferrite nanoparticles by polymer matrix templated synthesis
publisher Trans Tech Publications, Switzerland
publishDate 2010
url http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/
http://irep.iium.edu.my/16412/1/Preparation_of_Manganese_Zinc_Ferrite_Nanoparticles.pdf
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last_indexed 2023-09-18T20:25:13Z
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